GCMS unknowns report for sample AE12282, June 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\MAY2902\12282.D Vial: 23 Acq On : 30 May 2002 8:56 am Operator: Morgan Sample : gc/ms scan 5/23 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0528.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T.

14.68 1.47 ug/1 162982 Naphthalene-d8 15.70 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane,/ decamethyl- 370 C10H3005Si5 000541-02-6 80 2 Benzeneethanamine,/ N- (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 43 3 Benzeneethanamine, N- (pentafluorop 475 C21H26F5NO2Si2 055429-85-1 37 4 N-(Trifluoracet )-0,0‘,0"-tris(tri 495 C20H36F3NO4S13 000000-00-0 37 Abundance in 1049 (14.678 min): 12282.D (-) m/z 73.00 100.00% 73

5000 267 355 ■ 1 i ■ ■ • ■ i • ■ 14.40 14.60 14.80 15.00 45, 125154 193 223 1 ■ i ■ ■ ■ ■ i ■ rr. *** 1"J’t 11" . TTT323 , ■ ■ i ■ ■ ■ ■ i ■ ' ■ 1 i ■ ■ ■ ■ i ■ ■ m/z 266.95 33.27% miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 ■ ■ i ■ ■ ■ • i .......... I11 14.40 14.60 14.80 15.00 m/z 355.10 26.17% 207 a ■ i ■ ■ ■ ■ । ■ 1 1 ■ । ■ ■ ■ ' । ■ ■ ■ ■ f ■' 323 miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyl)methylene] 73 355 14.40 14.60 14.80 coo 5000 m/z 267.95 10.00%

45 208 251 281 | 386 458 548 ■ 11 1 • i ■ ■ ■ ■ i‘ ■ ■ ' i ■ ■ ■ ■ i ■ ■ ■ 1 i ■ ■ 1 ‘ 1 ■ '

mlz-> 50 100 150 200250300350400450500550 Abundance #74573: Benzeneethanamine, N-[(pentafluorophenyI)methylene] 73 14.40 14.60 14.80 15.00 m/ Z 74.00 9.18% 5000 267 44 , I, . 1 ’ 151179 209237 71**111111114 ■ 'i ■ ■ ■ ■ i • miz—> 50 100 150 200 250 300 350 400 450 500 550 1<40 14.60 14.80 15.00

12282.D GCMS0528.M Thu May 30 10:39:35 2002 Page 2

NYC-WTC_000013759