GCMS analysis results for sample AE12278, June 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\MAY2902\12278.D Vial: 19 Acq On : 30 May 2002 5:00 am Operator: Morgan Sample : gc/ms scan 5/23 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0528.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 14.68 2.16 ug/1 222821 Naphthalene-d8 15.70 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasaloxane, decamethyl- 370 C10H3005Si5 000541-02-6/ 80 / 2 Benzoic acid, 2-[(trimethylsilyl)ox 282 C13H2203Si2 003789-85-3 43 3 N-(Trifl roacetyl ) -N, O, O ' , O ’’-tetr 553 C22H42F3NO4Si4 000000-00-0 38 4 Benzenee hanamine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 38 Abundance 7 Scan 1049 (14.677 min): 12278.D (-) m/z 73.00 100.00% 73

5000 267 355 45 14.40 14.60 14.80 15.00 — TIB99 126 154 191 223 , , ——“mmTum 323 m/z 267.05 30.12% miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 5000 267 rr -J T 14.40 14.60 14.80 15.00 m/z 355.10 24.05%l ‘ 1 i 1 ■ ■ ■ i ■ • • • i ■ ■ —20— 323, m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #72298: Benzoic acid, 2-[(trimethylsilyl)oxy}-, trimethylsi 73 267

14.40 14.60 14.80 15.00 5000 m/z 74.00 8.36

135 193

mz-> 47 ' 11 ■ ' ■ ■ i ■ 50 100 11.001223/1../ 150 200 250 300 350 400 450 500 550 Abundance #60162: N-(Trifluoroacetyl)-N,O,O‘,O"-tetrakis(trimethylsi 73 14.40 14.60 14.80 15.00 m/z 356.10 8.26% 355 5000

45 — ii 147 193 267 538 ■ • l - ■ ■ • 'j ■ ■ ■ ■■ l ■ • • ■ l • r ' I 1 1 • ■ i ■ ■ ■ ■ i • ■ ■ 1 i ■ ■ ■ ■ i ■ ' ■ ■ i ' ' mfz~> 50 100 150 200 250 300 350 400 450 500 550 14.40 14.60 14.80 15.00

12278.D GCMS0528.M Thu May 30 10:38:37 2002 Page 2

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