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GCMS unknowns report for sample AE12280, June 2002

Machine-extracted title · confidence 100%

Report documenting analysis for unknown compounds and surrogate recovery in sample AE12280.

NYC-WTC_000013730–000013739

Folder label: “GCMS X 5/23/02 A 5/30/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\MAY2902\12280.D Vial: 21 Acq On : 30 May 2002 6:59 am Operator: Morgan Sample : gc/ms scan 5/23 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0528.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T.

14.68 1.58 ug/1 158552 Naphthalene-d8 15.70 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 72 2 3,4-Dihydroxybenzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 37 3 Benzeneethanamine, N-[ (pentafluorop 563 C24H34F5NO3S13 055429-13-5 37 4 N-(Trif/uoroacetyl)-0,0',0'1-tris(t 481 C19H34F3NO4Si3 000000-00-0 37 Abundance Scan 1049 (14.678 min): 12280.D (-) m/z 73.00 100.00% 73

5000 267 355 45 14.40 14.60 14.80 15.00 rrj108 fr* 223 , , Prim 193 r.T , 154 323 ■ ■ i ' ' ■ ' i 1 ■ ■ ■ i 1 ' 1 ■ i ■ 1 ■ 1 i ■ ■ ■ ■ i ' ■ m/z 266.95 32.08% mz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 14*40 14.60 14.80 '15'00 m/z 355.10 23.81%

74 .............. 207 323, mz-> 50 100 150 200 go 300 350 400 450 500 550 Abundance #49868:3,4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)- 73

267 14.40 14.60 14.80 15.00 5000 179 m/z74.00 9.73% 356 45

mz-> — 50 100 A Hr 300 350 400 450 500 550 150 147

200 209237, , 250 312 j..............................................

Abundance #74706: Benzeneethanamine, N-((perrtafluorophenyl)methylene] 73 355 1440 14.60 14.80 15'00 m/z 356.00 8.32% 5000

45 208 251 281 386 458 548 1 1 i • ■ i 11 1 ' n 1 ■ • i ■ ' 1 1 I '' 1 ' ' i ' ' 1 ' 1 r 1 T T T 50 100 150 200 250 300 350 400 450 500 550 14.40 1460 14.80 15.00

12280.D GCMS0528.M Thu May 30 10:39:05 2002 Page 2

NYC-WTC_000013738

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NYC-WTC_000013738Source: NYC Law Department, mirrored locally

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