GCMS calibration table data, sample AE09517, May 2002

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Library Search Compound Report Data File C:\HPCHEM\l\DATA\MAY0302\9517.D Vial: 18 Acq On 4 May 2002 6:43 am Operator: Sample GC/MS SCAN 4/22 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 14.79 0.54 ug/1 49160 Naphthalene-d8 15.83 Hit# of 5 .Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 72 2 3,4-Dihydroxybenzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 53 3 Benzeneethanamine, N-[ (pentafluorop 563 C24H34F5NO3S13 055429-13-5 38 4 N-(Trifl racetyl)-0,0',0"-tris(tri 495 C20H36F3NO4Si3 000000-00-0 28 Abundance Scan 1064 (14.793 min): 9517.D (-) m/z 73.10 100.00 73

5000 267 355 -

45 14,40 14,60 14.80 15,00 15.20 — —-*me 154 193 m/z 267.05 28.02%l m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 14.40 14.60 14.80 15.00 15.20 m/z 355.10 26.15 207 f 323, TT+ miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #49868:3,4-Dihydroxybenzyl alcohol,tris(trimethylsi)yl)- 73

14.40 14.60 14.80 15.00 15.20 5000 267 m/z 356.10 9.93 179 356 45 147

mz-> 4 50 209237, 1 ! ” 11 I 1 4— 312, + 100 150 200 250 300 350 400 450 500 550 C"l"k r i i . । i i

Abundance #74706: Benzeneethanamine, N-[(pentafIuorophenyl)methytene] 73 14.40 14.60 14.80 15.00 15.20 355 m/z 74.10 8.83 5000

45

miz—> 1501 ' 100 150 200208 251 281 TI"l ' ■ ' 1 i ' ' ' 250 300 386 458 548 i ’’ ' 1 ' { ''' H l ‘ 350 400 450 500 550 ' I ' ' ‘ ‘ I ■ ' ' ' I ‘ ‘ l"' I 1 ' 1 1 ! l' ' 14.40 14.60 14.80 15.00 15.20

9517.D GCMS0501.M Tue May 07 09:38:01 2002 Page 2

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