GCMS calibration table data, sample AE09517, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C: \HPCHEM\ 1 \DATA\MAY0 302\9517.D Vial: 18 Acq On 4 May 2002 6:43 am Operator: Sample GC/MS SCAN 4/22 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.16 10.13 ug/1 730624 1,4-Dichlorobenzene-d4 12.19

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 43 2 3-Hydroxy-2-pentanone 102 C5H10O2 003142-66-3 9 3 2,3-Butanedione, monooxime 101 C4H7NO2 000057-71-6 7 4 Propanenitrile, 3-ethoxy- 99 C5H9NO 002141-62-0 7 Abundance Scan 340 (8.158 min): 9517.D (-) m/z 43.05 100.00% 43

5000 59

101 7.80 8.00 8.20 8.40 8.60

miz-> 0*8** +53+ 10 20 30 40 50 60 70 69 83 I ■ • ■ • i ■ ' ' ■ i ' '■ 80 90 100 110 ...................... : /...............

Abundance #3245:2-Pentanone, 4-hydroxy-4-methyl- 43

5000 59 7.80 8.00 8.20 8.40 8.60 m/z 58.10 16.23% 31 83 101 1, TTT P4 73 I i ■ ■ ■ ' i ■ ■ ■ ■ i ' ' ' ‘ i ' - miz—> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1691:3-Hydroxy-2-pentanone 31 59 7.80 8.00 8.20 8.40 8.60 5000 m/z 101.15 12.70% 45 15 ,66 73 84 102 I ■ ■ ■ ■ i ■ ■ ■ ■ i ‘ 1 ' 1 I ‘ 1 ■ ■ i 1 ' ■ ‘ i • ■ ' i ■ ‘ ■ i ■ ■ • • i ■ ' ■ ■ i • 1 ■ i ■ ■ miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1607:2,3-Butanedione, monooxime .................. ;....... . ............ 43 7.80 8.00 8.20 8.40 8.60 m/ z 41.0.5 7.36%

5000

15 ' ■ i ■ ■ ‘ ■ i ■ .. 30 . 3,1 51 58...................... 191..... 1 • ‘ I ’ • ’ 1 I ‘ ‘ ’ ‘ I ’ ‘ 1 ‘ 1 1 ‘ ‘ 1 ’ ' ‘ • 1 * * 1 ’ 1 * memM / । TIP4 r m/z—> 10 20 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40 8.60

9517.D GCMS0501.M Tue May 07 09:38:00 2002 Page 1

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