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GCMS calibration table data, sample AE09517, May 2002

Machine-extracted title · confidence 90%

Calibration table listing response factors for deuterated standards and target compounds used in gas chromatography-mass spectrometry analysis.

NYC-WTC_000013117–000013125

Folder label: “GCMS X 5/21/02 A 5/21/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\MAYO 302\9517.D Vial: 18 Acq On 4 May 2002 6:43 am Operator: Sample GC/MS SCAN 4/22 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Anthracene-dlO- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 25.72 0.44 ug/1 39962 Phenanthrene-dl0 25.58

Hit# of 5 entative ID MW MolForm CAS# Qual 1 Anthracene-d10- 188 C14D10 001719-06-8 /94 2 Phenanthrene - dl 0 188 C14D10 001517-22-294 3 2-Quinolinecarboxaldehyde, 8-hydrox 188 C10H8N2O2 005603-22-5 42 4-(4-Toly])-3-methyl-pyrazol-5-one188C11H12N20 035496-19-6 38 Abundance Scan 2256 (25.716 min): 9517.D (-) m/z 188.15 100.00% 188

5000

mlz-> 40 52 -WH-H 6 A ! • • •' r ■ *11 •' " i 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 158 ( . fill... sssiman 25.40 25.60 25.80 26.00 m/z 189.15 16.97% Abundance #19957: Anthracene-d1 0- 188

5000 25.40 25.60 25.80 26.00 m/z 80.10 14.23% 66 80 94 •mmmmmmmmm 160

miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 118 T 25.40 25.60 25.80 26.00 5000 m/z 94.15 14.23%

80 94 160 66 TImmmTT m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #69165:2-Quinolinecarboxaldehyde, 8-hydroxy-, oxime 108 25.40 25.60 25.80 26.00 m/z 184.15 12.59%

5000

143 ............................................... 64 89 116 130 I. 158 170 m/z—> mfpmmbnju 1 Itr 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.40 25.60 25.80 26.00

9517.D GCMS0501.M Tue May 07 09:38:02 2002 Page 3

NYC-WTC_000013124

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NYC-WTC_000013124Source: NYC Law Department, mirrored locally

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