GC/MS analysis results, sample AE09581, May 2002

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Data File C:\HPCHEM\1\DATA\MAY0 302\9581.D Vial: 11 Acq On 3 May 2002 11:50 pm Operator: Sample GC/MS SCAN 4/24 FB Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 14.80 1.63 ug/1 143437 Naphthalene-d8 15.82

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 90 2 3,4-Dihydroxybenzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9—43 3 Benzeneethanamine, N- (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 38 4 Benzeneethanamine, N- (pentafluorop 475 C21H26F5NO2Si2 055429-85-1 37 Abundance Scan 1065 (14.797 min): 9581.D (-) m/z 73.05 100.00%| 73

5000 267 355 1 । 1 1 1 r । 1 1 45 14.40 14.60 14.80 15.00 15.20 I I । 125 154 193 223 323 I ‘ I ' ' 1 1 1 > 1 i I r‘ * )** "Ji i i r T i 7 r । | r i” i ) | i i i ITfui 1 r i- । । । । । i । । P r m/z 267.05 33 .89% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000- 14.40 14.60 14.80 15.00 15.20 m/z 355.10 33.55% ......... 207 323, TT+ n/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #49868: 3,4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)- 73 ■ ' i ' ' 14.40 14.60 14.80 15.00 15.20 267 m/z 356.10 11.39%) 5000- 179 ) 356 45 147 1 । । i । । । j । । । 14 r — — 209 237, 312 i m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyl)methylene] 7)3 14.40 14.60 14.80 15.00 15.20 355 m/z 268.05 8.92%

5000

m/z-> 45 . I , I 7 1 1 1 1 50 100 150 200 208 251 281 250 300 350 386 458 ‘ I**t‘I1III1TT 400 450 500 548 550 m. .. 14.40 14.60 14.80 15.00 15.20

9581.D GCMS0501.M Mon May 06 10:50:27 2002 Page 2

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