GCMS calibration table for sample AE09391, May 2002

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Technical document displaying GCMS calibration data and compound retention times for sample AE09391 processed in early May 2002.

NYC-WTC_000045452–000045461

Folder label: “GCMS X 5/3/02 A 5/8/02”

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NYC 9/11 Public Portal Document

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Data File C : \HPCHEM\ 1 \DATA\MAYO 102 \ 93 91. D Vial: 10 Acq On 1 May 2002 4:20 pm Operator: Sample gc/ms scan 4/18 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 14.80 0.53 ug/1 44176 Naphthalene-d8 15.84

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl - 370 C10H3005Si5 000541-02-6(83 2 3,4-Dihydroxybenzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 37 3 Benzeneethanamine, N- (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 28 4 Benzeneetha: .mine, N- (pentafluorop 475 C21H26F5NO2Si2 055429-85-1 25 Abundance Scan 1066 (14.805 min): 9391.D (-) m/z 73.10 100.00% 73

5000- 267 355 ....... n........ B i । । । k ।" । r । I । i~f—|-"i । । । । T

45 J54 193 ( | L 14.40 14.60 14.80 15.00 15.20 .1 .1 m/z 267.05 27.78% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 i 1 1 1 ' i 1 i 1 ' ‘ 1 i 1 1 14.40 14.60 14.80 15.00 15.20 m/z 355.10 26.85% 207 323 m/z-> 50 100 150 200 250 500 550 400 450 500 550 Abundance #49868: 3,4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)- 73 । । । > । । । । । । । । । । J■j । । । । [ । । 14.40 14.60 14.80 15.00 15.20 267 m/z 356.10 8.86% 5000 179 356 45 147 209 237, 312 1 1 i 1 1 T-T-j-r-r-r-i-y-r-r 1 I ’ ' 11 l' ' 1 mlz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyl)methylene] "di 73 14.40 14.60 14.80 15.00 15.20 355 m/z 74.10 8.65%| 5000-

45 208 251 281 386 458 548 । । । । । । । | । । । r । । f । । |' > । r i । । । । I[II i’i । t i r-1 1 i i r-1 i i d j । i m/z-> 50 100 150 200 250 300 350 400 450 500 550 14.40 14.60 14.80 15.00 15.20

9391.D GCMS0501.M Wed May 08 14:14:34 2002 Page 3

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