GCMS calibration table for sample AE09391, May 2002

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Technical document displaying GCMS calibration data and compound retention times for sample AE09391 processed in early May 2002.

NYC-WTC_000045452–000045461

Folder label: “GCMS X 5/3/02 A 5/8/02”

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Data File C:\HPCHEM\l\DATA\MAY0102\9391.D Vial: 10 Acq On 1 May 2002 4:20 pm Operator: Sample gc/ms scan 4/18 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Cyclotetrasiloxane, octamethyl Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 11.62 1.81 ug/1 118842 1,4-Dichlorobenzene-d4 12.21

Hit# of 5 Tentative ID MW MolForm CAS# Qual _____ Z__________ 1 Cyclotetrasiloxdne, octamethyl- 000556-67-2(9 296 C8H2404Si4 2 2-Oxo-4-pheny1-6- (4-chlorophenyl)-1 282 C16H11C1N20 000000-00-0 9 3 6,7-Benzo-phenothiazine-5,5-dioxide 281 C16H11NO2S 000000-00-0 9 4 Benzene, l-pnenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 9 Abundance Scan 718 (11.616 min): 9391.D (-) m/z 281.00 100.00% 281

5000

| > I I । | । > I T I- T—I " I | I I I I | I 1 I

43 59 73 87 103 119123 147 163 177 1?1 207 249 265 11.20 11.40 11.60 11.80 12.00 235 L L. ! ! | 'I1 ! , TTu0IBBB/“TnT 11 11 1 ' i'" ' i ' — ■ 1 i ‘ ■ 1 ■ i 1 11 ' i 1Tu —r m/z 282.00 27.34% rn/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #41966: Cyclotetrasiloxane, octamethyl- 281

5000 VTT J............... ■ 1 i 1 1 1 1 1 1 1 1 1 1 1 1 11.20 11.40 11.60 11.80 12.00 m/ z 283.00 17.32% ......... 73........... 1i.....163 177 191 207 235 249 265 I ‘ I il I l i i i i । i i I i । I । । i ll । । । । । । i । । । । i r‘ । i ill | I T I I | I I m | I I "i -Tri j—।—1—r

m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39756: 2-Oxo-4-phenyl-6-(4-chlorophenyl)-1,2-dihydropyrimi 281 1 ' I ' 1 11.20 11.40 11.60 11.80 12.00 5000 m/z 133.10 9.69%

102 123 141 175 204 247 1 1 i 1 ' ' 1 1 1 1 1 1 I ' 1 1 1 i 1 r 1 r i 1 1 1 1 i ■ ■ ' ■ i 1 1 1 ' । 17 -i । ।’t । । । । । । ' । | । '■ i > । । । । । [H‘ - m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39602: 6,7-Benzo-phenothiazine-5,5-dioxide Tk 281 11.20 11.40 11.60 11.80 12.00 m/z 265.05’ 7.67% A 5000

217 232 102 ns 189 204 1.1 252264 7 I I 1 I 1 1 — I | I I !' 1 | I IIIInnIIIIII-IIIIItIIIIIi 1 i ri । 1 i i I । i i । i pi r i 1 1 1 1 i J TUT m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 11.20 11.40 11.60 11.80 12.00

9391.D GCMS0501.M Wed May 08 14:14:33 2002 Page 2

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