Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
NYC-WTC_000004149–000004492Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2701\30708.D Vial: 49 Acq On : 30 Dec 2001 6:21 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L
Peak Number 3 Cyclotetrasiloxane, octamethyl Concentration Rank 12
R.T. EstConc Area Relative to ISTD R.T.
11.13 0.98 ug/1 456298 1,4-Dichlorobenzene-d4 11.67
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclotetrasiloxane, octamethyl- 000556-67-2 87 296 C8H24O4Si4 2 2-Oxo-4-phenyl-6- (4-chlorophenyl)-1 282 C16H11C1N2O 000000-00-0 9 3 6,7-Benzo-phenothiazine-5, 5-dioxide 281 C16H11NO2S 000000-00-0 9 4 Benzene, 1 -phenyl-4- (2-cyano-2-phen 281 C21H15N_____ 027869-56-3 9 Abundance / Sran 663 (11,133 min): 30708.D 6 m/z 281.00 1 00.00% 281
5000
45 59 73 89 103 119 133 147 163 177 123 207 221 235 249 265 10.80 11.00 11.20 11.40 IIostav • < । । 1 । i । 'i । j " i’*i 17 । 1 T 1 1 1''r 1 । ""1 1 i' lhi । 'i1 r 1 j c 1 । । 'r । j । "1 1 । । "1 1 j । r m/z 282.00 2 9.57% m/z~>40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #41966: Cyclotetrasiloxane, octamethyl- 281
5000 10.80 11.00 11.20 11.40 ' ' 1 207 m/z 283.00 17.75% 73 133 1411/+/*/A1‘‘‘‘1/‘‘‘‘I‘/‘/‘14L,"/I111+/114"1‘IEI I 163 177 1?,1 -X , । , , 235 . , । 249 265 I । । । CTT m/z-> 40 60 80_ 100 120 140 160 180 200 220 240 260 280 Abundance #39756. 2-Oxo-4-phienyl-6-(4 -chlorophenyl)-1 2-dihydropyrimi 281 ........ ) T’ l | • 1 I > |
10.80 11.00 11.20 11.40 5000 m/z 192.90 11.40%
102 123 141 175 204 247 m/z-> 40 60 80 100 120 140 160 180 200 " 220 240 260 280 Abundance #39602: 6,7-Benzo-phenothiazine-5,5-dioxide 1 ' I 1 1 ■ 1 1 281 10.80 11.00 11.20 11.40 m/z 133.00 10.41% | 5000 217 232 102 118 189 204 III 252264 । ■ ■ 1 ' ■ ■ ■ | ' > • - | ‘ l'1 I ■ ! 1 ) > | ■ . I I | 1 ! I I | 1 I1'! I | I I 1" I । । ri । 1 1 > 1 । । 1 । 1 fi 1 1 1 I 1 1 1 1 I 1 r T4 11148 1 m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 10.80 11.00 11.20 11.40
30708.D GCMS1126.M Mon Jan 28 11:28:27 2002 Page 3
NYC-WTC_000004342
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NYC-WTC_000036712
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Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
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GCMS analysis report for sample AD29523 listing unknown compounds and surrogate recovery data from January 28, 2002.
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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD303B5 conducted on January 10, 2002.
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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30251 conducted on January 9, 2002.
1 shared topics · similarity 0.997
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Laboratory report noting contamination from the TurboVap concentrator and recovery rates for sample AD28662.
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28479 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034180
Laboratory report detailing GCMS analysis of sample AD28269 conducted on November 30, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034213
Laboratory report detailing GCMS analysis of sample AD28271 conducted on December 6, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.996
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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033765
Analytical commentary for sample AD28149 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034819
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000004148
Fragmented OCR text showing dates and identifiers for a DEP GCMS record dated February 2002.
Filed in the same folder
NYC-WTC_000036712
GCMS analysis report for sample AD29563 listing unknown compounds and surrogate recovery data from January 28, 2002.
Similar indexed content
NYC-WTC_000018546
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
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NYC-WTC_000036798
GCMS analysis report for sample AD29523 listing unknown compounds and surrogate recovery data from January 28, 2002.
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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD303B5 conducted on January 10, 2002.
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