Instrument log and analysis summary for GCMS testing of sample AE09676 conducted on May 23, 2002.
NYC-WTC_000023789–000023810Folder label: “GCMS X 5/9/02 A 5/20/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\l\DATA\MAY2002\9676.D Vial: 10 Acq On : 20 May 2002 4:02 pm Operator: Sample : EXTRACTED 5/9 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 3 Cyclotetrasiloxane, octamethyl Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 11.55 1.31 ug/1 72501 1,4-Dichlorobenzene-d4 12.14 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 9 2 6,7-Benzo-phenothiazine-5,5-dioxide 281 C16H11NO2S 000000-00-0 9 3 3,6-Bis(N-dimethylamino)-9-ethylcar 281 C18H23N3 057103-04-5 9 4 Benzene, l-p>lenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 9 Abundance T Scan 711 (11.552 min): 9676.D (-) m/z 281.00 100.00% 211
5000
Id 43 59 73 87 103 119133 163177 191 207 249 265 11.20 11.40 11.60 11.80 TtIudoDTDHummmmTTTTr 1 1 i' ■i„ ■ 11 1L. ■ ‘ i —r m/z 282.00 29.42% mz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #41966: Cyclotetrasiloxane, octamethyl- 201
- 5000 11.20 11.40 11.60 11.80 m/z 283.00 17.93% 133 207 73 ' I ‘ ‘ ' 1 I ' ' ' 1 1 1 ' 1 1 1 1 I 163 177 191 ' i 1 1 ■ ' i ■ r ■ ■ i ■ ■ 1 '' i ■ 1 ■ ‘ i ' L 235 249 265 , || , miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39602:6,7-Benzo-phenothiazine-5,5-dioxide 281 ............... I 1 ■ i ' 1 ■ ■ i ■ ■ ' 1 ■ ■ i ■ ■ ■ ' i ■ 11.20 11.40 11.60 11.80 5000 m/z 133.10 11.96% 217 232 102 118 189 204
mlz-> ’1 1’1’1111’’I41/111’/1’’1/1/1’’111’’I’’/1I" 11 ’ I 40 60 80 100 120 140 160 180 200 1.14/111/1252264.. 220 240 260 280 , Abundance #39624:3,6-Bis(N-dimethylamino)-9-ethylcarbazole i ■ ' ■ 11 281 11.20 11.40 11.60 11.80 m/z 73.10 9.89% 5000 266
141 208 222 237250 TTTTTTTP-np-hpTT 1 i ■ ‘ ‘ 1 i 1 ■ ■ 1 i ■ 1 1 ■ i ' m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 11.20 11.40 11.60 11.80
9676.D GCMS0520.M Tue May 21 11:39:16 2002 Page 3
NYC-WTC_000023798
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NYC-WTC_000023649
Laboratory report showing GC/MS blank analysis for sample AE09676 with non-detect results for volatile organic compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039588
Laboratory report documenting GCMS analysis of sample AE06455 conducted on April 19, 2002, by the DEP.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005394
Laboratory report listing unknown compounds and surrogate recovery data for sample AE02604.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009835
Calibration data for GCMS analysis using 625/TCLP method with deuterated compound reference standards recorded on February 21, 2002.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038871
Laboratory report documenting GCMS analysis of sample AE02575 conducted on March 25, 2002, identifying other unknown compounds.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039497
Laboratory report documenting GCMS analysis of sample AE06449 conducted on April 19, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005415
Laboratory report listing unknown compounds and surrogate recovery data for sample AE02645.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039469
Laboratory report documenting GCMS analysis of sample AE06430 conducted on April 19, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005367
Laboratory report showing non-detectable results for nitrosamines and chlorinated solvents in GCMS blank.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047979
GCMS analysis report for sample AE05749 showing surrogate recovery and unknown compounds from April 2002.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013943
TCLP calibration table document dated May 24, 2002, listing deuterated standards and response factors for GCMS analysis.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039611
Laboratory report documenting GCMS analysis of sample AE06456 conducted on April 19, 2002, by the DEP.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000023646
Department of Environmental Protection administrative record sheet for World Trade Center site activities dated May 2002.
Filed in the same folder
NYC-WTC_000023647
Technical data file header page from a GCMS analysis run associated with the World Trade Center site in May 2002.
Filed in the same folder
NYC-WTC_000023649
Laboratory report showing GC/MS blank analysis for sample AE09676 with non-detect results for volatile organic compounds.
Filed in the same folder
NYC-WTC_000023662
Laboratory report showing GC/MS calibration data for volatile organic compounds analyzed on May 20-21, 2002.
Filed in the same folder
NYC-WTC_000023666
Laboratory report showing GC/MS reference analysis for sample AE09676 with quantitative results for volatile organic compounds.
Filed in the same folder