Instrument log and analysis summary for GCMS testing of sample AE09676 conducted on May 23, 2002.
NYC-WTC_000023789–000023810Folder label: “GCMS X 5/9/02 A 5/20/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\l\DATA\MAY2002\9676.D Vial: 10 Acq On : 20 May 2002 4:02 pm Operator: Sample : EXTRACTED 5/9 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Cyclopentasiloxane, decamethyl Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 14.75 1.54 ug/1 109670 Naphthalene-d8 15.78 Hit# Of 5 entative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl - 370 C10H30O5S15 000541-02-6 90 2 N- (Trifluoroacetyl) -0,0' ,0' 1 -tris (t 481 C19H34F3NO4Si3 000000-00-0 28 3 Benzoic acid, 2,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 28 4 Benzeneethanamine, N-[ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 28 Abundance Scan 1060 (14.751 min): 9676.D (-) m/z 73.10 100.00% 73
5000
267 355 _ 45 14.40 14.60 14.80 15.00 108 133154 193 223 323 .k........................ ‘ 'i 1 I i ■ t 1''' ■ ‘*15 " । ' ■■ ■ ' T ' ' i ■ ■ ■ 1 i 1 ' 1 ' i ' m/z 266.95 24.30% m/z-> 50 100 150 200 250 300 350 400 450 Abundance #51266: Cyclopentasiloxane, decamethyl- 73
355 267 5000 TT 14.40 14.60 14.80 15.00 m/z 355.10 24.09% .............................. 207 323 ■ 1 i m/z-> 50 100 150 200 250 300 350 400 450 Abundance #58326: N-(Trifluoroacetyl)-O,O',O”-tris(trimethylsilyl)no 73
355 14.40 14.60 14.80 15.00 5000 m/z 356.10 8.27%
45 . I , I |, 126147 193 ‘ ‘i ' ‘ ' ‘II*’II I * III * 265 376 481 miz-> 50 100 150 200 250 300 350 400 450 Abundance #73978: Benzoic acid, 2,5-bis(trimethylsiloxy)-, trimethyls ...................... ,........................... 73 14.40 14.60 14.80 15.00 355 m/ Z 74.10 8.11% 5000-
45 ,147 179 223 , 267 297 ...................... ,,............................ 1 m/z-> 50 100 150 200 250 300 350 400 450 14.40 14.60 14.80 15.00
9676.D GCMS0520.M Tue May 21 11:39:17 2002 Page 4
NYC-WTC_000023799
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NYC-WTC_000023649
Laboratory report showing GC/MS blank analysis for sample AE09676 with non-detect results for volatile organic compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039588
Laboratory report documenting GCMS analysis of sample AE06455 conducted on April 19, 2002, by the DEP.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005394
Laboratory report listing unknown compounds and surrogate recovery data for sample AE02604.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009835
Calibration data for GCMS analysis using 625/TCLP method with deuterated compound reference standards recorded on February 21, 2002.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038871
Laboratory report documenting GCMS analysis of sample AE02575 conducted on March 25, 2002, identifying other unknown compounds.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039497
Laboratory report documenting GCMS analysis of sample AE06449 conducted on April 19, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005415
Laboratory report listing unknown compounds and surrogate recovery data for sample AE02645.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039469
Laboratory report documenting GCMS analysis of sample AE06430 conducted on April 19, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005367
Laboratory report showing non-detectable results for nitrosamines and chlorinated solvents in GCMS blank.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047979
GCMS analysis report for sample AE05749 showing surrogate recovery and unknown compounds from April 2002.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013943
TCLP calibration table document dated May 24, 2002, listing deuterated standards and response factors for GCMS analysis.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039611
Laboratory report documenting GCMS analysis of sample AE06456 conducted on April 19, 2002, by the DEP.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000023646
Department of Environmental Protection administrative record sheet for World Trade Center site activities dated May 2002.
Filed in the same folder
NYC-WTC_000023647
Technical data file header page from a GCMS analysis run associated with the World Trade Center site in May 2002.
Filed in the same folder
NYC-WTC_000023649
Laboratory report showing GC/MS blank analysis for sample AE09676 with non-detect results for volatile organic compounds.
Filed in the same folder
NYC-WTC_000023662
Laboratory report showing GC/MS calibration data for volatile organic compounds analyzed on May 20-21, 2002.
Filed in the same folder
NYC-WTC_000023666
Laboratory report showing GC/MS reference analysis for sample AE09676 with quantitative results for volatile organic compounds.
Filed in the same folder