GCMS analysis results for sample AE06429, April 23, 2002

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Library Search Compound Report Data File : C:\HPCHEM\l\DATA\APR1202\6429.D Vial: 12 Acq On : 15 Apr 2002 6:51 pm Operator: Sample : re-extract Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 14.83 0.49 ug/1 80624 Naphthalene-d8 15.86 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 58 2 3,4-Dihydroxybenzyl alcohol, tris (tr 356 C16H3203Si3 068595-79-9 52 3 N- (Trifluorcacetyl) -N, 0,0’ ,0* ′-tetr 553 C22H42F3NO4Si4 000000-00-0 35 4 Benzeneethanamine, N-[ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 32 Abundance Scan 1065 (14.825 min): 6429.D (-) m/z 73.00 100.00% 73

5000 267 355 ....... H ........ 14.40 14.60 14.80 15.00 15.20 45 adili 125.154, *F1931*‘ 3.237 1323 1+1**I****1**‘4I****1****I****1** m/z 267.00 42.10% mz-> 50 100 150 200250300350400450500550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 14.40 14.60 14.80 15.00 15.20 m/z 355.05 37.79% ----2 50 100 150 200 250 323, mlz-> 300 350 400 450 500 550 Abundance #49868:3,4-Dihydroxybenzyl alcohol,tris(trimethylsily!)- 73 ■j-n-r-r-p-r ‘ ‘ I ' ' ' ‘ I ' ' 14.40 14.60 14.80 15.00 15.20 5000 267 m/z 356.05 14.87% 179

45 147 356 ft — 209237, 312 ' ' I ° —T ■ i 1 ■ ' 1 i ■ ■ ■ i ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i 1 ■ ■ ■ i ' 1

miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60162: N-(Trifluoroacetyl)-N,0,O’,0"-tetrakis(trimethylsi । i ■ ■ i । । » ■ ■ i ■ ■ ■ ■ i ■ ■ 73 14.40 14.60 14.80 15.00 15.20 m/z 268.00 10.89% 355 5000-

45 | 1) 147 193 267 538 T miz—> 50 100 150 200250300350400450500 550 14.40 14.60 14.80 15.00 15.20

6429.D GCMS0412.M Tue Apr 16 15:42:01 2002 Page 2

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