GCMS analysis results for sample AE06429, April 23, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\APR1202\6429.D Vial: 12 Acq On : 15 Apr 2002 6:51 pm Operator: Sample : re-extract Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Anthracene-dlO- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 25.75 0.25 ug/1 45362 Phenanthrene-dl0 25.61 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 50 2 Phenanthrene-dlO 188 C14D10 001517-22-2 47 3 Antipyrine 188 C11H12N2O 000060-80-0 45 4 Naphthalene, 1,7-dimethoxy- 188 C12H1202 005309-18-2 45 Abundance Scan 2255 (25,750 min): 6429.D (-) m/z 188.10 100.00% 188

5000

25.40 25.60 25.80 26.00 44 66 80 94 160 L m/z 189.10 13.42% 1’3 /z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d1 0- 1118

5000 ■ ■ i ■ ■ r ' I ‘ ‘ • 1 I 1 1 1 ' I 1 25.40 25.60 25.80 26.00 m/z 94.00 12.33% 80 94 160 66 1 ■ i ■•■ ■ i • "■ i ■ ■ 1 ■ i H “ 1111 ■ I “ " I " ■' l" 1' 11 “ ‘ 11"11"' nfe-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 1118 **1**’)’*314’ 1I* 25.40 25.60 25.80 26.00 5000 m/z 184.05 12.14%

94 80 160 66 - I H ' 111111 ........I*.... mfe-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance . .i । i । । । । i i i । । । #19872: Antipyrine 118 25.40 25.60 25.80 26.00 96 m/z92.00 8.61%

5000 77 56 105

iz—> 1111" ।1 40 50 • i “ “ i■ 60 70 80 T+ 4 159 173 TOOUIBUOumPT ILT 90 100 110 120 130 140 150 160 170 180 190 25.40 25.60 25.80 26.00 ‘ ‘

6429.D GCMS0412.M Tue Apr 16 15:42:02 2002 Page 3

NYC-WTC_000048836