GCMS analysis results for sample AE05852, April 23, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\APR1202\5852.D Vial: 7 Acq On : 15 Apr 2002 1:57 pm Operator: Sample : re-extract Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Anthracene-dlO- Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 25.75 0.24 ug/1 46568 Phenanthrene-dl0 25.61 Hit# of 5 ./Tentative ID MW MolForm CAS# Qual 1 Anthracene/dlO- 6 188 C14D10 001719-06-8 2 Phenanthrene -d10. 188 C14D10 001517-22-2 3 Pentacyclo[8.4.0.0(3,7).0(4,14).0(6 188 C14H20 000000-00-0 36 4 4H-Pyri [1,2-a]pyrimidin-4-one, 3- 188 C11H12N2O 057773-19-0 28 Abundance Scan 2256 (25.754 min): 5852.D (-) m/z 188.10 100.00% 188

5000

1 49,172... 1.... 1.... 1..,....,...,,...... ...... 1....... 4 266 80 94 .. u 156 T 25.40 25.60 25.80 26.00 m/z 189.10 T

17.73% }iT

mk-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d10- 1118

.._____ 5000 25.40 25.60 25.80 26.00 m/z 184.10 14.87%! —FFpFF,HpHL-pprrprpFGPA—AL iz—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 188 4| 25.40 25.60 25.80 26.00 5000 m/z 79.95 14.34%

m 80 94 160 0** 66 i “' ■ i • ■ “ i mfz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19959: Pentacyclo[8.4.0.0(3,7).0(4,14).0(6,11)tetradecane 118 25.40 25.60 25.80 26.00 m/z 94.00 10.73

5000 79 92 . _ 117 .. 106 । 131 145 159 173 .... /............. 1 ■ ■ i ■ ■" i ■ ■" i ■ ■ ■ ■ i'1 - ...... 1.....1..... IU’T, . I ■ ' . r I 1 । ° I 1 1 1 1 I 1 1 1 1 I 1 m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.40 25.60 25.80 26.00

5852.D GCMS0412.M Tue Apr 16 15:40:37 2002 Page 4

NYC-WTC_000048747