GCMS calibration data, Sample 1647, Mar 2002

Machine-extracted title · confidence 100%

Calibration table for GC/MS analysis using Method 625/TCLP recorded on March 12 and 19, 2002.

NYC-WTC_000012200–000012206

Folder label: “GCMS X 3-1-02 A 3-20-02 MANY RERNNS”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAR1102\1647.D Vial: 23 Acq On : 12 Mar 2002 12:53 pm Operator: Sample : re-ext fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Anthracene-dlO- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

25.83 0.21 ug/1 31297 Phenanthrene-dl0 25.70

Hit# of Tentative ID 5 MW MolForm CAS# Qual / .2_. 1 Anthracene-diO 188 C14D10 001719-06-8 94 2 Phenanthrene 188 C14D10 001517-22-2 91 3 Naphthalene, 188 C12H1202 005309-18-2 42 4 4H-Pyrido [1,/ -a]pyrimidin-4-one. 3- 188 C11H12N2O 057773-19-0 40 Abundance Scan 2264 (25.826 min): 1647.D (-) m/z 188.10 100.00% 188

5000-

66 80 94 158 42 " i" i h 1111 111 — 25.40 25.60 25.80 26.00 26.20 "'I1'"i1 “'i111‘i" ‘11111' 111 ■ ■ * ■ i ■ ■ ■ ■ t ■ • ■ ■ i1 " • i “ m/z 189.05 14.65% m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance" #19957: Anthracene-d IQ- 188

5000 25.40 25.60 25.80 26.00 26.20 m/ z 93.95 14.26% 66 80 94 160 " I'1 “ 1111' i " ।r i1 " ‘ I “ "'I ।'11111111'1'11 “1 ■ i1 ■ “ i “ “ i “ 1 ■ I ■1 “ I “ 3’3 miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance j 10069* Dhepgnthrene-d10 188 25.40 25.60 25.80 26.00 26.20 5000 m/z 184.05 11.92%

80 160 66 7 94 TTmPPTm, •11 ■ । • ■ ■ ■ ।1 ■ ■ ■ i “ ‘ । ■ ■ ■ ■ । ■1 • i ■ ■ ■11 ■ ■ ■ ■ । ' TrT m/z->____ 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance ~ #19913: Naphthalene, 1,7-dimethoxy- 173 188 25.40 25.60 25.80 26.00 26.20 m/z 158.05 11.84%

5000 115 145 102 51 63 130 75 158 94 । ■ • i “ ' • f' ‘1' i 1 TTIUI] 1' 111'' 11' 1111 1 F rri prrprr ITT “i ■ ■ i ■'1 ■ i'1 ■ ■ i ‘ ■1 m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.40 25.60 25.80 26.00 26.20

1647.D GCMS0308.M Tue Mar 19 09:15:37 2002 Page 1

NYC-WTC_000012205

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