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GCMS analysis results for sample AE05846, April 23, 2002

Machine-extracted title · confidence 100%

GCMS laboratory report for sample AE05846 analyzed on April 23, 2002, by analyst DLV.

NYC-WTC_000048717–000048736

Folder label: “GCMS X 4/11/02 A 4/15/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\APR1202\5846.D Vial: 6 Acq On : 15 Apr 2002 12:59 pm Operator: Sample : re-extract Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Anthracene-dlO- Concentration Rank 3

R.T. EstConc Area Relative to I STD R.T. 25.75 0.25 ug/1 52317 Phenanthrene-dl0 25.61

Hit# of 5 'entative ID MW MolForm CAS# Qual

1 Anthracene-diO- , 188 C14D10 001719-06-8 2 Phenant hrene - dl 057 188 C14D10 001517-22-2 3 4-Methyl-2-y (3-f luorophenyl) pyrimidi 188 C11H9FN2 076128-66-0 42 4 4-Methyl-2/(4-fluorophenyljpyrimidi 188 C11H9FN2 Abundance Scan 2255 (25.750 min): 5846.D (-) 188 m/ z ] 10 J 076128-67-1 42

5000

80 42 52 64 94 158 1 ITT 25.40 25.60 25.80 26.00 '11 “■i1'" i'11‘i1‘1n1 mT+ | m/z 79.95 14.86%| mz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d1 0- 188

5000 ■ ■ i ■ ■ 25.40 25.60 25.80 26.00 m/z 189.10 12.42%| 80 94 160 66 mz-> ■ ■ I ■ ■ ■ ■ I ■' 111' I i ■ I

40 50 60 70 80 " i " ■' i ■ ■ ■ ■ i" ■ ■ i' ■ “ i ■ 90 100 110 120 130 140 150 160 170 180 190 ......I..... Abundance #19958: Phenanthrene-d10 188

25.40 25.60 25.80 26.00 ‘ ‘ 5000 m/ z 93.90 11.64%|

80 94 160 66 m/z-> 0 40 50 60 hasp Mn p i i ■ । i i i i । i ■ ! i |-n r r-| i . I 70 80 90 100 110 120 130 140 150 160 170 180 190 . ..... W... Abundance #19859:4-Methyl-2-(3-fluorophenyl)pyrimicline ,............... 158 25.40 25.60 25.80 26.00 m/z 184.10 11.23%| 5000 121

173 671 75 (5 ____ 94|, "I‘ ' i " " I " 111" " I'1 " 111 " I " 1111 „ |.. 146 161 I.. । 1111111 ■।111'I''1' 111" I " " I " " 11111 I’T 7 y m/z—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.40 25.60 25.80 26.00

5846.D GCMS0412.M Tue Apr 16 15:40:13 2002 Page 3

NYC-WTC_000048726

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NYC-WTC_000048726Source: NYC Law Department, mirrored locally

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