GCMS analysis results for sample AE05852, April 23, 2002

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\APR1202\5852.D Vial: 7 Acq On : 15 Apr 2002 1:57 pm Operator: Sample : re-extract Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ****************************************************** * ************** Peak Number 3 Heptadecane Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 23.92 0.28 ug/1 55390 Phenanthrene-dl0 25.61 Hit# of 5 Tentative ID MW MolForm CAS# Qual A 1 Heptadecane 240 C17H36 000629-78-7 97 2 Eicosane 282 C20H42 000112-95-8/91 3 Pentadecane 212 C15H32 000629-62-9 91 4 Octadecane 254 C18H38 000593-45-3 91 Abundance Scan 2056 (23.918 min): 5852.D (-) m/z 57.0,0 100.00% 57 43 71 5000 85 . । . . 7 । / W f — > ■, 23.60 23.80 24.00 24.20

m/z-> 4 ill.L • ‘ i ■ ■, . L” ^7?^ ........................... 40 60 80 100 120 140 160 180 200 220 240 260 280 m/z 43.05 72.39% Abundance #71193: Heptadecane 57

71 mA. | 1M । , fA | 5000 85 23.60 23.80 24.00 24.20 m/z 71.00 62.94% 1. 113 127 141 155 169,2020 . mfa-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance 43 5 7

71 #72323: Eicosane

..... /W.... 23.60 23.80 24.00 24.20 ' 5000 m/z 85.05 41.89% 85

— ....................................................................... . miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance 57 #26001: Pentadecane A ‘ * 1 ‘ ‘ 4 I ’ A Ar.... 23.60 23.80 24.00 24.20 43 71 m/z 41.05 35.87

5000 85

99 4.9 * • t • • 1 113 127 ....... 168......... 212.................. • ns.AAAA TIB At 1’ ' i *’141+1141’1*’1**’*14*’*141*1++I’++I+’’I+I ... m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 23.60 23.80 24.00 24.20

5852.D GCMS0412.M Tue Apr 16 15:40:36 2002 Page 3

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