GCMS analysis results for sample AE06427, April 23, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\APR1202\6427.D Vial: 11 Acq On : 15 Apr 2002 5:52 pm Operator: Sample : re-extract Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 14.83 0.33 ug/1 58258 Naphthalene-d8 15.87 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 59 2 N-(Trifluordacetyl)-0,0’,0''-tris(t 481 C19H34F3NO4S13 000000-00-0 37 3 Phenethylamine, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 37 4 Benzoic aci , 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 37 Abundance / Scan 1066 (14.830 min): 6427.D (-) m/ z 73.00 100.00% 73

5000 267 355

45 14.40 14.60 14.80 15.00 15.20 108133154 ,193 223 1 । ■ ■ i ■ 323 m/z 267.00 47.17% 1 1 1113 1 1 ■ • i ′ ■ • ■ i ■ ■ ■ ■ i ■ ■ miz-> 50 100 150 200 250 300 350 400 450 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 ....... . ...... .. 5000 267 14.40 14.60 14.80 15.00 15.20 m/z 355.05 45.13% .27 323 |......... miz-> 50 100 150 200 250 300 350 400 450 Abundance #58326: N-(Trifluoroacety!)-O,0‘,0"-tris(trimethylsilyl)no 73 /

355 T T T 14.40 14.60 14.80 15.00 15.20 5000 m/z 356.05 18.10%

45 | It 126147 193... 265 ....... 376 481 miz—> 50 100 150 200 250 300 350 400 450 Abundance #74239: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethyls i ■ ■ ■ ■ i ■ ‘ ■ • i ' • ‘ ' i ■ • 73 14.40 14.60 14.80 15.00 15.20 m/z 267.90 12.26% 5000 355 44

m/z—> _L ’ 4 I * ‘ 50 100 147 150 193 200 250 267 294 300 | 350 400 450 14.40 14.60 14.80 15.00 15.20

6427.D GCMS0412.M Tue Apr 16 15:41:45 2002 Page 2

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