GCMS sample AE07110 results, April 25, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\APR2202\7110.D Vial: 20 Acq On : 23 Apr 2002 3:41 am Operator: Sample : re-ext Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

14.81 0.49 ug/1 85066 Naphthalene-d8 15.84

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02- 2 N- (Trifluoroacetyl)-N,O,O’,0' ’-tetr 553 C22H42F3NO4Si4 000000-00- 3 3,4-Dihydroxybenzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 46 4 Phenethylamine, N-methyl-.beta. ,3,4 399 C18H37NO3Si3 010538-85-9 38 Abundance Scan 1063 (14.808 min): 7110.D (-) m/z 73.00 100.00% 73

5000 267 355

14.40 14.60 14.80 15.00 15.20 45 i > • * i ' ‘ 108133 162 193.223 , , 323 | m/z 355.05 42.87% mfe-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 i ■ ■ • ■ i ‘ ■ 14.40 14.60 14.80 15.00 15.20 m/z 267.00 41.06%

11 i ’ .2 1 | * 323, « | | B< • • "II i"i i i । i । i r [ t i । i । i i

mtz~> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60162: N-(Trifluoroacety!)-N,0,0’,0"-tetrakis(trimethylsi 73 |.................. . ........................ 355 14.40 14.60 14.80 15.00 15.20 5000 m/z 356.05 15.65%

45 I 147 193 267 538 * ‘i ■ ■ • * i 1 * * ‘ i 1 * * * i ‘ * 1 • i ‘ ■ i ■ ‘ ■ i ■ ■ ■ ■ i 1 1 1 ' I ‘ ■ i ■ 111 t m&—> 50 100 150 200 250 300 350 400 450 500 550 Abundance #49868:3,4-Dihydroxybenzyl alcohol, tris(trimethylsilyl)- .................... i ■ ■ ■ ■ i ■ ‘ ■ i • • i ■ 1 ' ■ i ■ ■ 73 14.40 14.60 14.80 15.00 15.20 m/z 267.90 12.52% 267 5000 179 356 45 147

z—> +4 50 100 4 150 209 237, < ■ l" 200 250 312 dr *‘1*‘‘‘I*‘‘I**‘‘I‘***I*‘‘‘I** 300 350 400 450 500 550 = 14.40 14.60 14.80 15.00 15.20

7110.D GCMS0412.M Tue Apr 23 14:22:47 2002 Page 2

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