GCMS sample AE07110 results, April 25, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\APR2202\7110.D Vial: 20 Acq On : 23 Apr 2002 3:41 am Operator: Sample : re-ext Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 8.19 6.74 ug/1 906108 1,4-Dichlorobenzene-d4 12.21 Hit# of 5 Tentative ID MW MolForm CAS# Qual 12-Pentanone,/ 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 50 2 Acetic acid, cyano-, 1,1-dimethylet 141 C7H11N021 001116-98-9 17 3 Morpholine/ 4-methyl- 101 C5H11NO 000109-02-4 9 4 Butane, 1/ethoxy- 102 C6H140 000628-81-9 9 Abundance Scan 342 (8.189 min): 7110.D (-) m/z 42.95 100.00%| 43

59 5000

101 ,..... . 7.80 8.00 8.20 8.40 8.60 374 +53+ 71 83 I ■ • ■ ■ i ■ 1 1 ■ I 1 ■ ■ ■ i ■ ' ■ 111 • ■ ■ i ■ • • ■ i • ■ • 1 i ■ ■ m/z 59.05 53.32? miz-> 10 20 30 40 5060 70 80 90 100 110 120 130 Abundance #64275: 2-Pentanone, 4-hydroxy-4-methyl- 43

5000 59 7.80 8.00 8.20 8.40 8.60 m/z 101.05 22.01%l 15 31 — 101 I t TTT 1 " I i ■ ■ ■ ■ i ■ 1 ■ 1 i 83 | • ■ i ■ ■ ■ 1 i ■ • ■ • i ■ ■ • • 1 ■ ' ■ ■ i • ' mlz~> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #7666: Acetic acid, cyano-, 1,1 -dimethylethyl ester 59 7.80 8.00 8.20 8.40 8.60 5000 41 m/z 58.05 16.78? 68 • ■ । ‘ । ■ • ■ • । ‘ ■ 1 1" ____________________126 miz-> 10 20 30 40I 50 60 70 80 90 100 110 120 130 ____ Abundance #1640: Morpholine, 4-methyl- TTmnnpnim 43 7.80 8.00 8.20 8.40 8.60 m/z 41.05 7.79? 5000 101 15 71 27 ----- -Tm— i 56 I t miz—> 10 20 30 40 50 60 70 80 90 100 110 120 130 7.80 8.00 8.20 8.40 8.60

7110.D GCMS0412.M Tue Apr 23 14:22:46 2002 Page 1

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