GCMS sample analysis report AE05844, Apr 18 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\APR1202\5844.D Vial: 20 Acq On : 16 Apr 2002 2:42 am Operator: Sample : re-extract Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.20 5.22 ug/1 677904 1,4-Dichlorobenzene-d4 12.23

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 50 2 Acetic acid, cyano-, 1,1-dimethylet 141 C7H11N02 001116-98-9 17 3 CH2=CHCH2v(0)OCH3 100 C5H802 003724-55-8 10 4 Morpholine, 4-methyl-__________ 101 C5H11NO 000109-02-4 9 Abundance Scan 344 (8.201 min): 5844. D (-) m/ z 42.95 100.00% 43

59 5000-

101 7.80 8.00 8.20 8.40 8.60 ■ ' i 1 ................. 37 h ' i' 1 1 1 ' 1 ) 1 53. Hi ' Petr 69 3 / m/z 59.05 52.10% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #64275: 2-Pentanone, 4-hydroxy-4-methyl- 43

5000 59 7.80 8.00 8.20 8.40 8.60 m/z 100.95 21.36% 15 31 101 I i 83 | ■ ■ । ■ ■ ■ ■ । ■ ■ ■ ■ । • TTH TP—H m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #7666: Acetic acid, cyano-, 1,1-dimethylethyl ester 59 7.80 8.00 8.20 8.40 8.60 5000 41 m/z 58.05 16.59%

68 126 PPTTTTTI.. . — 10 20 30 40I 50 (60 70 80 90 100 110 120 130 Abundance #1448: CH2=CHCH2C(O)OCH3 ' i 1 1 4(3 7.80 8.00 8.20 8.40 8.60 m/ z 41.05 7.60%

5000

58 ..... ...... | 72 ioo ■ i ■ ■ ■ ■ t > ■ ■ ■ । > < । 1 । । 1 i 1 ‘ 1 ' i ' 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 7.80 8.00 8.60

5844.D GCMS0412.M Wed Apr 17 09:47:15 2002 Page 1

NYC-WTC_000048519