GCMS instrument log for sample AE09676, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\l\DATA\MAY2002\9676.D Vial: 10 Acq On : 20 May 2002 4:02 pm Operator: Sample : EXTRACTED 5/9 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Acetone Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 9.92 0.95 ug/1 52367 1,4-Dichlorobenzene-d4 12.14 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetone 58 C3H60 000067-64-1 9 2 S- (-) -Methylbutylamine 87 C5H13N 020626-52-2 7 3 4-Pe: ten-2-one, 4-methyl- 98 C6H10O 003744-02-3 7 4 5-He, en-2-one 98 C6H10O 000109-49-9 5 Abundance Scan 533 (9.921 min): 9676.D (-) m/z 43.05 100.00%| 43

5000

58 87 | 98 39 39 51 । | 69 9.60 9.80 10.00 10.20 mmPmPPPmmmm m/z 58.10 21.57%I m/z—> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #62322: Acetone 43

5000 9.60 9.80 10.00 10.20 58 m/z 87.00 14.47%| 27 msgollaggt । | 1 1 1 1 | 1 1 1 1 | 1 1 । | । । । । | । । । । | । । M | !!! I | ! I I I | ! I I I | I ! I ! | | | | | | | | ,! | , | m/z—> 15 20 25 30 35 . 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #764: S-(-)-2-Methylbutylamine 33 ' ' I ' ■ ' ‘Il i । । । > । । । । 9.60 9.80 10.00 10.20 5000 m/ Z 59.10 13.58%|

,41 56 70 87 ''" ।" i'1'111" ■ i" ■111'" i" ■ ■ i" " 1111 ■ i" " i11" i1"11" " r" " i'11111 “11 “ " i" " i" m/z—> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1244:4-Penten-2-one, 4-methyl- ■ ‘ i 1 ■ 1 1 i ■ 1 ' 1 i ' ■ ■ ■ i 43 9.60 9.80 10.00 10.20 m/ z 41.10 9.98%

5000

A 83 M 29

m/z—> . .... ”..............?............... 1....... 1.... 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 MAAA 9.60 9.80 11111 1‛III 10.00 10.20

9676.D GCMS0520.M Tue May 21 11:39:14 2002 Page 2

NYC-WTC_000023797