GC/MS analysis results, sample AE10605, May 10 2002

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAY1002\10605.D Vial: 7 Acq On : 10 May 2002 6:55 pm Operator: Sample : GC/MS SCAN 5/9 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 l-Propen-2-ol, acetate Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

10.33 1.15 ug/l 90842 1,4-Dichlorobenzene-d4 12.17

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Propen/2-ol, acetate 100 C5H802 000108-22-5 9 2 Pentane/ 3-ethyl- 100 C7H16 000617-78-7 9 3 Acetic Acid, pentyl ester 130 C7H14O2 000628-63-7 9 4 5-Hexen-2-one 98 C6H10O 000109-49-9 9 Abundance 7 Scan 578 (10.334 min): 10605.D (-) m/z 43.05 100.00% 43

5000 70 TI 84 99 112 127 10.00 10.20 10.40 10.60 49 55 ------ -1- rn/ Z 70.05 28.41% ' ' i l'1'1 ' i ' ' ' ■ I ' ' ' ' i 1 • ' ' I ' ' J ' ' miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #1477:1-Propen-2-ol, acetate 43

5000 *‘111111*’’‘ I’‘ ‘I‘ ‘I 10.00 10.20 10.40 10.60 m/z 39.10 9.19% 58 72 527371 ...... 1.... J 1 1 I 1 ' 1 1 I 1 1 1 1 I ■ ■ ' 1 1 1 10 20 30 40 50 60 70 100 miz-> 80 90 100 110 120 130 Abundance #63426: Pentane, 3-ethyl- 43 IMA/yAAmn/ 10.00 10.20 10.40 10.60 5000 71 m/z 99.1.0 7.69%

27 55 ' I ' 1 ' 1 1 ‘ 437 ■ i ■ ■ ■ ■ i 1 |..................... 100............................ miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #65234: Acetic acid, pentyl ester 43 10.00 10.20 10.40 10.60 m/z 41.15 7.18%

5000

mlz-> 27 ....... 7... . —L _7 10 20 30 40 50 55 61

60 70

70 80 90 100 110 120 130 A10.00 10.20 10.40 10.60

10605.D GCMS0510.M Mon May 13 09:31:53 2002 Page 3

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