GC/MS analysis results, sample AE10605, May 10 2002

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\MAY1002\10605.D Vial: 7 Acq On : 10 May 2002 6:55 pm Operator: Sample : GC/MS SCAN 5/9 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 1-Pyrrolidineethanamine Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

13.48 4.68 ug/1 370893 1,4-Dichlorobenzene-d4 12.17

Hit# of 5 . Tentative ID MW MolForm CAS# Qual

1 1-Pyrrolidineethanamine 114 C6H14N2 007154-73-6 38 2 Aziridine, 2-methyl-3-(1-methylethy 99 C6H13N 010027-95-9 37 3 Cyclopentanone, 2-(1-methylpropyl) - 140 C9H160 006376-92-7 25 4 1-Dodecanone, 1-cyclopropyl-_____ 224 C15H280 019873-44-0 25 Abundance 7 Scan 921 (13.477 min): 10605.D (-) m/z 84.10 100.00% . 84 42

5000 126 141 98

miz-> 10 20 30 40 ,50.11—44. l 50 58

60 70

70 80 90 112 "i...... 11 1 1 1 1 ।11' 1 i 1 100 110 120 130 140 m/z 13.20 13.40 13.60 13.80 42.0.5 69.46% Abundance #2949:1-Pyrrolidineethanamine 84

42 5000 13.20 13.40 13.60 13.80 30 m/z 126.15 39.07% 56 70 I 114 miz-> 10 20 30 ‘ it I. I.. I.. i ■111 ■ ■11' ■'1 i1 ‘1 ■ i ■ ■'11'1 ■11''1 11 ■ 40 50 60 70 80 90 100 110 120 130 140 Abundance #1422: Aziridine, 2-methyl-3-(1 -methylethyl)-, trans- 84 V "IT 13.20 13.40 13.60 13.80 5000 m/ z 44.05 34.98% 27 44 56 15

mz-> ’ 1’1 10 -PP ' ■ i ■ 1 199 ' ' i ' ■ ■ ■ i ■ ■ ■ ■ i ■' ■ ■ i 1 ' ■ ■ i ‘ ■ i' ' ■ ■ i ■ 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #7511: Cyclopentanone, 2-(1-methylpropyl)- 84 13,20 13.40 13,60 13.80 m/z 41.05 24.15% 5000 55

69

n/z-> 11 ■ ■ ■ ■ i ■111111'' i' 10 20 30 40 — 50 60 470 — 96 ’IT TIPT 111 140 IH 80 90 100 110 120 130 140 i' ■ ■11 11 1 [ 1 1 1 * [ ' 1 13.20 13.40 13.60 13.80

10605.D GCMS0510.M Mon May 13 09:31:54 2002 Page 4

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