GCMS analysis results for sample AE11602, June 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\MAY2102\11602.D Vial: 31 Acq On : 22 May 2002 8:06 pm Operator: Sample : EXTRACT5/20 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P g**

Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 14 Cyclopentane, 1,3-dimethyl-, c Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 13.35 6.90 ug/1 442738 1,4-Dichlorobenzene-d4 12.15 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentane, 1,3-dimethyl -, cis- 98 C7H14 002532-58-3 43 2 Acetic cid, octyl ester 172 C10H20O2 000112-14-1 42 3 5-Azul' emethanol, 1,2,3,3a, 4,5,6,7 222 C15H260 055255-90-8 38 4 Cyclopentane, 1,3-dimethyl-, trans- 98 C7H14 001759-58-6 38 Abundance 7 Scan 906 (13.346 min): 11602.D (-) m/ z 43.05 100.00% 43 56

5000 70 83 AAL 13.00 13.20 13.40 13.60

nlz-> — 20 30 4 40 +50 50 +TT 60 70 .,77 I 80 TIf ■ ■ I1 98 105 115 125 112010——n/m—mB[Bn 90 100 110 120 130 m/z 56.10 67.77% Abundance #63267: Cyclopentane, 1,3-dimethyl-, cis- 41 56 70

5000 27 13.00 13.20 13*40 13.60 ‘ ‘ ' 83 m/z 55.10 36.78%

„,A, 98 PPH 1 1 i ■ 1 ■ • i ■ 1 niz—> 20 30 40 50 00 70 80 90 100 110 120 130 Abundance #15763: Acetic acid, octyl ester 43 "* i 1 13.00 13.20 13.40 13.60 5000 56 70 m/z 70.05 28.40% 84 112 97 I

AW ■ • i ■ ■ 1 1 i • • ■ 1 i ' • 1 1 i 1 ' ' ' I ' ' 1 I ■ ■ ■ ■ i 1 ' 1 ' 1 • i * * miz-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #28209:5-Azulenemethanol, 1,2,3,3a,4,5,6,7-octahydro-.alph 43 13.00 13.20 13.40 13.60 58 m/z 41.05 27.94% 5000 70 85 92

• i ' ‘ ■ ■ i ' 1 ' ' I ‘ I’ 98 _ 106 113........... ■ 1 I ■ ■ 1 ■ i ■ 1 1 ' i ■ ■ ■ ■ i ■ ■ - /z—> 20 30 40 50 60 70 80 90 100 110 120 130 13.00 13.20 13.40 13.60

11602.D GCMS0520.M Fri May 24 08:33:17 2002 Page 14

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