GCMS analysis results for sample AE01462, Feb 2002

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Data File : C:\HPCHEM\1\DATA\FEB2102\1462.D Vial: 15 Acq On : 22 Feb 2002 3 :53 am Operator: Sample : gc/ms scan 1/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2,4-Dimethyl-1-heptene Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

8.22 1.18 ug/1 109194 1,4-Dichlorobenzene-d4 12.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2,4-Dimethyl-1/-heptene 126 C9H18 019549-87-2 50 2 Heptane, 3-methylene- 112 C8H16 001632-16-2 47 3 Cyclopentane, 1,2,3-trimethyl-, (1. 112 C8H16 002613-69-6 42 4 Undecane, 3 zmethylene- 168 C12H24 071138-64-2 42 Abundance 7 Scan 346 (8.222 min): 1462.D (-) m/ z 43.05 100.00% 43 70

5000 55

83 TTP Pr r 7.80 8.00 8.20 8.40 8.60 4449+4 — 103 126 ■ । ' ■ j 1 i ■ j ' 1 1 1 ■ । ■ i 1-1 1 • i । ’ l 1 • • > [ • ■ m/z 70.00 70.41% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #4662: 2,4-Dimethyi-1-heptene 43 70 55

5000 83 7.80 8.00 8.20 8.40 8.60 27 m/ z 73 . 0 54.70% I 126 —————— • ■ i • • 1 I ' 1 m/z- 20 30 40 50 60 70 80 90 100 110 120 .130 Abundance C . ■ - 0 : ■

55 70 1 7.80 8.00 8.20 8.40 8.60 5000 m/z 55.00 48.54% 42 27 112 83 ■ । ■ •' ■ i ■ 1 ' 1 i ' 1 ■ ' i 1 ■ ' ' i ' ' ■ 1 i ' ' ■ ' i ..................... ... . , . i i . । । i । > । i > i । । i < miz-____ 20__ 30 _ Abundance 40 50 60 70 80. 90 100 110 #2714: Cyclopentane, 1,2,3-trimethyl-, (1.aipha.,2.aipha., 70 120 130 ,.. Aw I ' ' ' ' I ' ' ' ' I ' ' ' 1 I 7.80 8.00 8.20 8.40 8.60 55 m/ z 41.0,5 46.20% 5000 41

27 84 L - 97 112 m/z-> ' j • ■ ■ ■ i ■ ■ 1 ■ I 20 30 40 1 1 i ■ ■ 50 1 60 70 80 ■ ' I • < 90 ■ i * .................... ....... 100 110 120 130 -IP8.00- 7.80 8.20 8.40 8.60

1462.D GCMS0308.M Mon Mar 25 08:27:25 2002 Page 3

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