GCMS analysis results for sample AE10890, May 2002

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Data File : C:\HPCHEM\1\DATA\MAY1502\10890.D Vial: 8 Acq On : 15 May 2002 8:55 pm Operator: Sample : GC/MS SCAN 5/10 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 2 1-Heptene, 4-methyl- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 7.79 1.59 ug/1 88851 1,4-Dichlorobenzene-d4 12.16 Hit# of Tentative ID MW MolForm CAS# Qual

1 1-Heptene, 4-methyl- 112 C8H16 013151-05-8 38 21, 6-Heptadien-4-ol 112 C7H120 002883-45-6 25 3 4-Pentenal 84 C5H80 002100-17-6 25 4 1-Butanol, 2,3-dimethyl-_________ 102 C6H140 019550-30-2 25 Abundance Scan 300 (7.788 min): 10890.D (-) m/z 41.05 100.00% 41

5000- 69 /

• i ‘ 1 1 ' i ■ l ' '~ pi । i । । । । 53 58 84 7.40 7.60 7.80 8.00 8.20 -3H +47-HHHm TTTTTTTTTTTTTTTTT m/ z 43.05 70.74% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 Abundance #2675:1-Heptene, 4-methyl- 43 70

5000 55 7.40 7.60 7.80 8.00 8.20 27 m/z 69.05 46.32%

mlz-> l v ‘I’TmpTP 84 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 ____________ 112 i' ■'11 ■ ■ ■ ■ i11" i' ■" i' ■ ‘ ■ i ■ ■ ■r i'

Abundance #2591:1,6-Heptadien-4-ol 43 1. h g 71 7.40 7.60 7.80 8.00 8.20 5000 m/z 39.10 45 .98% 27 53 79 Tyuuni) Hmmm iTTTrTTTYTTTTpTTTpTTTpTTTTrTTTp^^

4 "r i" " i' mz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 Abundance #571:4-Pentenal 23 41 55 7.40 7.60 7.80 8.00 8.20 m/ Z 71.10 40.15% 5000

83 . . . 1. .... 49 49 _....... |........... 11' i" " i1 ' 11"' i ‘1 ‘ i " i ■ ■" i" ' "1 r "' i" " i" " i"' ■ i" 111"1111111'1 ri i11" i11111" " i11" i' ) ? । , , P. । . . m/z—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110115 120 7.40 7.60 7,80 8.00 8.20

10890.D GCMS0510.M Fri May 17 10:07:38 2002 Page 2

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