GCMS unknown compound analysis, sample AE05515, April 2002

NYC 9/11 Public Portal Document

■ f Library Search Compound Report

Data File C:\HPCHEM\l\DATA\APR0102\5515.D Vial: 6 Acq On 1 Apr 2002 4:11 pm Operator: Sample gc/ms scan 3/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L *************** *********************************** ******************* Peak Number 7 1-Heptene, 5-methoxy-4-methyl- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

10.00 1.18 ug/1 198906 1,4-Dichlorobenzene-d4 12.25

Hit# of 5 'entative ID MW MolForm CAS# Qual

1 1-Heptene, S-methoxy-4-methyl- 142 C9H18O 054004-21-6 9 2 Propane, 2ymethoxy-2-methyl- 88 C5H12O 001634-04-4 9 3 2-Methyl-^hexen-3-ol 114 C7H14O 032815-70-6 9 4 3,5-Dimet/iyl-5-hexen-3-ol 128 C8H16O ^00000-^02° 5 Abundance Scan 540 (10. min): 5515.D(-) m/z.. 73.00 " 100.00%

5000 43 57 137

151 9.60 9.80 10.00 10.20 10.40 -yE 93 1" ‘ 'I*''' m/z; 43.00 38.12% ___ 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #66199: 1-Heptene, 5-methoxy-4-methyl- 73

5000 —r-Z 9.60 9.80 10.00 10.20 10.40 45 81 m/z 136.95 34.42% 27 59 rT-iT-i-rm-TTVi-T-i-i^^ 100 ,I m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #62937: Propane, 2-methoxy-2-fnethyl- 73

9.60 9.80 10.00 10.20 10.40 5000 m/z 57.00 33.44% 57 41 ■15 27 I I'''' I T nn/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #3017: 2-Methyl-5-hexen-3-ol 713 9.60 9.80 10.00 10.20 10.40 55 m/z 138.95 33.11% 43 5000

27 It - ' I' I' I ■ I' 11' " ' I.. •' I ■p’ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 9.60 9.80 10.00 10.20 10.40

5515.D GCMS0403.M Thu Apr 04 13:53:16 2002 Page 7

NYC-WTC_000059330