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GCMS analysis results for sample AE04131, April 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of environmental sample AE04131 conducted on April 1, 2002.

NYC-WTC_000011817–000011832

Folder label: “GCMS X 2/25/02 A 3/23/02

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Scanned page image, NYC-WTC_000011830
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAR2202\4131.D vial: 27 Acq On : 23 Mar 2002 9:42 pm Operator: Sample : gc/ms scan 2/25 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ******************************************************* ** ************ Peak Number 7 3,5-Dimethyl-5-hexen-3-ol Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

10.01 2.05 ug/1 234795 1,4-Dichlorobenzene-d4 12.26

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3,5-Dimethyl-5-hexen-^-ol 128 C8H160 000000-00-0 9 2 Octanal, 7 -methoxy-3, 7 -dimethyl - 186 C11H2202 003613-30-7 9 3 3,4-Dimethyl-5-hexfen-3-ol 128 C8H160 000000-00-0 9 4 2 -Methyl - 5 -hexen-3-ol 114 C7H140 032815-70-6 8 Abundance Scan 541 (10.013 min): 4131.D (-) m/z 73.0,0 100.00% 73

5000 43 57 137 IT 1IMII’II t-t-j-t-t 151 9.60 9.80 10.00 10.20 10.40 1 m/z-> ..... 20 30 40 50 60 , 85 95 109 121 11 TIT TK)umwanmpT I..,. 1’*.. I.... 1.... I 70 80 90 100 110 120 130 140 150 160 170 m/z 43.00 39.28% Abundance #5017: 3,5-Dimethyl-5-hexen-3-ol 73 43

5000- 55 TTTTT7 ■ 9.60 9.80 10.00 10.20 10.40 27 m/z 57.0,0 35.42% .81 99 ■ i1 ■ ■ ■ i ■ ■ ■ ‘ i ■ •' ■ i ■' ■ ■ i ■ ■ l l'l1 -4*I’A’AISAA+I***+L++++I-A*SI*ASSGAUSSSAA*/*| miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance £19455 Octana 7rkd : • eth 73 —ITTTT 9.60 9.80 10.00 10.20 10.40 5000 m/z 136.95 35.03%

42 55 81 95 121 171 m/z--> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170"1T Abundance #5018:3,4-Dimethyl-5-hexen-3-ol ***I**’I*V[111144 73 9.60 9.80 10.00 10.20 10.40 m/z 138.95 33.78% 43 5000 55

27 ---TTT , 81 99 I" | ‘ ‘ I■ ' I ‘" ' ! “ “I ■ ‘"! " "! ‘ ‘ ' I ' ' "i “"I" ' ' I m/z->_ 20 30 40 50 60 70 „ 80 90 100110 120 130 140 150 160 170 9.60 9.80 10.00 10.20 10.40

4131.D GCMS0308.M Wed Mar 27 10:10:13 2002 Page 7

NYC-WTC_000011830

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NYC-WTC_000011830Source: NYC Law Department, mirrored locally

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