GCMS analysis results for sample AD29783, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report i

Data File : C:\HPCHEM\l\DATA\DEC1401\29783.D Vial : 6 Acq On 15 Dec 2001 7:25 am Operator: 209 GALOS Sample : gems scan 12/10 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 3,4-Dimethyl-5-hexen-3-ol Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

9.45 1.00 ug/1 290991 1,4-Dichlorobenzene-d4 11.67

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 3,4-Dimethyl-5-hexen-3-ol 128 C8H160 000000-00-0 12 2 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 3 Propane, 2-methoxy-2 -methyl- 88 C5H120 001634-04-4 9 4 1.beta.,4/Xi.-Guaian-11-ol_________ 224 C15H280 028892-33-3 9 Abundance 7 Scan 480 (9.448 min): 29783.D (-) m/ z 73.0,0 100.00% 73

5000 43 55 137

151 9.20 9.40 9.60 9.80 35 | I, | , ,| , 83 95 109 123 11 > TT’TITT T TTTTT । T । । — TIT’r TTI’nur i1'1 TT ‘I’’ m/ 43.00 36.82% m/z--> 10 20 30 40 50 60 70 80 90 '100 110 120 130 140 150 160 Abundance #5018: 3,4-Dimethyl-5-hexen-3-ol 73

43 5000- 55 9.20 9.40 9.60 9.80

27 m/z 54.95 34.34% I; H— .............. 99 irr.rp ‘‘111111-111I it m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #62932: Silane, tetramethyl- 73 / ——————— 9.20 9.40 9.60 9.80 5000- m/ z 34.06%

45 15 J 53 j 88 ■ । ■1 ■■ i ■ ■■' । i ■TTTTttttttttTTgr i1''' i'''11'' ■ • i ■''' i'1 * • i TT m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #62967: Propane, 2-methoxy-2-methyl- r 'I ' ' ' ' l ''I • IT=IP 73 9.20 9.40 9.60i 9.80 m/z 136.95 33.54% 5000 - 57 41 15 27... 11 1111 1 111 TI + mPPP । . Y. r|r. . . । ■ r i | i ■ . > ] ■ . > । । < > ■ ■ । m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 9.20 9.40 9.60 9.80

29783.D GCMS1126.M Fri Dec 28 13:16:02 2001 Page 8

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