GCMS analysis results for sample AD29783, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1401\29783.D Vial: 6 Acq On 15 Dec 2001 7:25 am Operator: 209 GALOS Sample : gems scan 12/10 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Butane, 1,3-dibromo-3-methyl- Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

11.07 0.61 ug/1 178210 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butane, 1,3-dibromo-3-methyl- 228 C5H10Br2 024443-15-0 42 2 Pentane, 1,4-dibromo- 228 C5H10Br2 000626-87-9 38 3 Pentane, 2,4-dibromo- 228 C5H10Br2 019398-53-9 38 4 1-Pentene/ 5-bromo- 148 C5H9Br 001119-51-3 37 I Abundance Scan 657 (11.072 min): 29783.D (-) m/z 41.05 100 00% 41 69 149

5000 55

109 121 10.80 11.00 11.20 11.40

m/z-> .... ■ ।11 20 +1 148414 —634 80 - I-IPIIIIFIIITTIT 30 40 50 60 70 80 90 100 110 120 130 140 150 m/ z 69.10 74.61% Abundance #29403: Butane, 1,3-dibromo-3-methyl- 41 69

5000 149 10.80 'A 11.00 11.20 1 11.40 '

27 53 m/ z 14 8.90 70.21% 80 95 107 123 133 m/z-> "‘I‘ 20 TTTTumuuuuuumworit 30 40 50 60 70 80 90 100 110 120 130 140 H 150 Abundance #29407: Pentane. 1,4-dibromo- 41 69 • ' 1 1 ' • 1 I ■ ' i ■ • ' ■ i ' ■ 10.80 11.00 11.20 11.40 5000 27 m/z 150.9,0 69.50%

149 53 80 95 107 i 1 I TIT 1 i ■ 1 ' ■ i ' ■ i 111 1 i 1 ' 1‘ 1 T miz--> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #29405: Pentane, 2,4-dibromo- i • ■ ■ ■ i ' ' 41 69 10.80 11.00 .11.20 11.40 m/z 39.0,5 41.77% 5000- 27

m/z—> —PP I, 20 30 40 50 53 I । 1 i ■ ■ ■ ■ i ■ '

60 80 109 । | 170" ' 80h 1 1 ■90।'■■■100। ■ ‘ 110T । । 120।।। 151 II .।.... । 130 140 150 CTf 10.80 11.00 .N 11.20 11.40

29783.D GCMS1126.M Fri Dec 28 13:16:12 2001 Page 9

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