GCMS unknown compound analysis, sample AE05515, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\APRO102\5515.D Vial: 6 Acq On 1 Apr 2002 4:11 pm Operator: Sample gc/ms scan 3/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 Butane, 1,3-dibromo-3-methyl- Concentration Rank 8

R.T. . EstConc Area Relative to ISTD R.T.

11.65 0.59 ug/1 99316 1,4-Dichlorobenzene-d4 12.25

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butane, ^3-dibromo-3-methyl- 228 C5H10Br2: 024443-15-0 43 2 Pentane/ 1,4-dibromo- 228 C5H10Br2; 000626-87-9 35 3 Pentan^, 2 ,'4-dibromo- 228 C5H10Br2: ' 019398-53-9 25 . 4 2-Pentene, 4-bromo- 148 C5H9Br 001809-26-3 16

■±2 Slundanc^ Scan 720 (11.652 min): 5515.D (-) 41 69 151

ux 5000 55 81 107 121133 281 11.40 11.60 11.80 12.00 n It I I m/z 151.0.0 87.46% Ti/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280. Abundance #294'03: Butane, 1,3-dibromo-3-methyl- 41

5000 149 I \ 11.40 11.60 11.80 12.00 27 53 m/z 86.71% I ' I ' ' ' ' I ' ,82 95 IO/ 123135 , m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #29407: Pentane. 1,4-dibromo- 4'1 69 i 11.40 11.60 11.80 12.00 5000 27 ra/z 148.9n 83.05%

, I 53 • 82, 95 1?7 ................. •n/z->__ 20.__40__ 60__ 80 100' 120 140 160 180 200 220 240 260 280 Abundance #29405: Pentane', 2.4-dibrom’o-"".... 2. 4i1 6|9 11.40 11.60 11.80 12.00 m/z 39.0,5 38.39% 5000 27

151 53 109 81 il II m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 11.40 11.60 11.80 12.00

5515.D GCMS0403.M Thu Apr 04 13:53:21 2002 Page 8

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