GCMS sample AE05062 analysis, April 2002

NYC 9/11 Public Portal Document

Library ’Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR3002\5056.D Vial: 32 Acq On : 30 Mar 2002 11:42 pm Operator: Sample : gc/ms scan 3/8 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ★******************************************************************** Peak Number 1 Butane, 2-methoxy-2-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.14 0.79 ug/1 99386 1,4-Dichlorobenzene-d4 12.25

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butane, 2-methoxy-2-methyl- 102 C6H14O 000994-05-8 33 2 N-Ethylformamide 73 C3H7NO 000627-45-2 9 3 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 __4 Pentane, 3 -methoxy- 102 C6H14O __ 036839-67-5 9 'Abundance Scan 337 (8.138 min): 5056.D (-) m/z 73 OQ ioo7oo% ! 7|3 i

5000- 43

87 103 7.80 8.00 8.20 8.40 .33,1, I 49 I ' ' ' ' I ' ' ' ' I ' ,57r'Y"r-i-i— , I ' ' 80 ' 'go 'l6o ' 110 m/ z 43.05 , 29.09% Wz->10 20 30 40 50 I60 70 Abundance #1761: Butane, 2-methoxy-2-methyl- 713

5000 i 7.80 8.00 8.20 8.40 55 87 m/ z 41.05 10.09% 45 ......... 27 33 ' ' I ' ' ' ' I ' ' ' ' I ' ' I ' I ' ' ' ‘ I ' ' ' ' I I SO ' ' 'go' ' 100 'iio ___ 10 20 30 40 50 60 70 l^bundance ifZW.: N-Ethylformarnide i 30 73 A fAA ... 7.80 8.00 8.20 8.40 5000 m/ z 45.05 9.07% 44 58 15 ; • 'm/z-> 10 20 30 40 _ 50 60 70 80___ 90 100 110 Abundance #M5: Silane, tetramethyl- 713 7.80 .,..O....... 8.00 8.20 8.40 1 m/z 71.00 7.55% 5000 A 15 55 I 88 I Va 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40

5056.D GCMS0308.M Tue Apr 02 15:34:01 2002 Page 1

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