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← Document results/DEP Box 22/GCMS X 11/24/01 A 12/4/01
Document / 12 pages

GCMS analysis comments for sample AD28662, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report noting contamination from the TurboVap concentrator and recovery rates for sample AD28662.

NYC-WTC_000034988–000034999

Folder label: “GCMS X 11/24/01 A 12/4/01”

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Scanned page image, NYC-WTC_000034994
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV2601\28680.D Vial: 11 Acq On : 28 Nov 2001 3:03 am Operator: 209 GALOS Sample : 11/24 scan Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Butane, 2-methoxy-2-methyl- Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 7.64 1.16 ug/1 251500 1,4-Dichlorobenzene-d4 11.69 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Butane, 2-methoxy-2-methyl- 102 C6H140 000994-05-8 36 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 3 N-Ethylformamide 73 C3H7NO 000627-45-2 9 4 Pentane ,/3-methoxy- __________ 102 C6H140 036839-67-5 9 Abundance ' Scan 282 (7.637 min): 28680. D (-) m/z 73.00 100.00% 73

5000

43 — I • ' • ■ i ' 7.20 7.40 7.60 7.80 8.00 ‘ I I I 55 i 87 103 TITTCTITIETTTUTIITTTTTTTTT’IT 207 m/z 43.05 23.91% ?nfz~> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #1761: Butane, 2-methoxy-2-methyl- 73

5000 ----- ----- 7.20 7.40 7.60 7.80 8.00 55 87 m/z 41.05 10.17% 45 27 11111" i11 111111 ml 1 r "' i T‘TUII"TUIOCIOIEUIOCCUTICEUIUTCCTOOTTTTTT‘T‘‘T miz—> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #62932: Silane, tetramethyl- 73 MAAAPIAPPT 1IT4 7.20 7.40 7.60 7.80 8.00 5000 m/z 44.95 9.40%

45 THTTT4.88 15 I 55 TTTTT i1■i>i>••• i > • ■ ■ i ■ ■ • ■ । ■ i >■•>।> <■>।■>■•। m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #292: N-Ethylformamide T’ATTTT 33 7.20 7.40 7.60 7.80 8.00 73

5000- 44 58

15 I ' < 1 < । ■ 1 -.......... m/z—> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 7.20 7.40 7.60 7.80 8.00

28680.D GCMS1126.M Thu Dec 06 13:13:04 2001 Page 1

NYC-WTC_000034994

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NYC-WTC_000034994Source: NYC Law Department, mirrored locally

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