Laboratory report noting contamination from the TurboVap concentrator and recovery rates for sample AD28662.
NYC-WTC_000034988–000034999Folder label: “GCMS X 11/24/01 A 12/4/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV2601\28680.D Vial: 11 Acq On : 28 Nov 2001 3:03 am Operator: 209 GALOS Sample : 11/24 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1,4-Dichlorobenzene-d4 Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 11.57 0.50 ug/1 108330 1,4-Dichlorobenzene-d4 11.69 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1, 4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 53 2 Benzene-1,2,3, 4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 25 3 Benzonitrile, 2 amino-5-chloro- 152 C7H5C1N2 005922-60-1 9 4 Benzofuran, 7-chloro- 152 C8H5C1O ____ 024410-55-7 9 Abundance 7 Scan 710 (11.566 min): 28680.D (-) Tm/z 149.90 100.00% 150
5000 115 78 - 52 38 87 1120 11.40 11.60 11.80 -H-H • ■ i ■ 3. 40 50 60 70 80 90 100 110 120 —l i.TTT 1 1— m/z 151.90 61.14% mz-> 30 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 150 *
5000 115 ............. ... ).................... 1120 11.40 11.60 11.80 52 78 m/z 114.90 34.99% 87 rnfz~> 30 35 ' • i •' • ■ i ■ ■ ' • i 40 50 111'1 ■ ■ 11 ■ 60 70 -PP ... ....... I 80 90 100 110 120 130 140 150 160 I—— Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 150 TP — 1 i 1 115 1120 11.40 11.60 11.80 5000 52 78 m/z 78.05 . 21.26%
35 87
miz-> 30 L 40 50 11 I 1 1 1 1 1 1 1 60 I i '' 1 11 ■' ' ■ i' ’ ' ’ i ■ ■ 70 80 90 100 110 120 130 140 150 160 1........ Abundance #10109: Benzonitrile, 2-amino-5-chloro- ............. -............. 152 11.20 11.40 11.60 11.80 m/z 52.00 15.58% 5000 125 63 90 117 I 98 ................ ........... .... ■ । ‘ 11 11 ■ ■ • i ■ i ■ ■ I ■ • ■ ■ i ■ • ■ ■ । m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80
28680.D GCMS1126.M Thu Dec 06 13:13:07 2001 Page 2
NYC-WTC_000034995
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Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.
NYC-WTC_000034886
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28479 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034808
Laboratory analyst notes on GCMS scan results, recovery rates, and low pH conditions for sample AD28649.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034819
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034198
Laboratory report detailing GCMS analysis of sample AD28263 conducted between November 21 and 26, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034180
Laboratory report detailing GCMS analysis of sample AD28269 conducted on November 30, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034213
Laboratory report detailing GCMS analysis of sample AD28271 conducted on December 6, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034830
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034331
Laboratory report documenting GCMS analysis of sample AD28427 conducted between November 21 and 26, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033765
Analytical commentary for sample AD28149 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033834
Analytical commentary for sample AD28155 dated November 29, 2001, noting detection of bis(2-Ethylhexyl)phthalate and low recovery rates.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000004149
Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033800
Analytical commentary for sample AD28157 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000034946
Laboratory report detailing GCMS scan results for sample AD28650, noting phthalate detection and low pH.
Filed in the same folder
NYC-WTC_000034947
Document containing unreadable text or corrupted data from the Department of Environmental Protection archives.
Filed in the same folder
NYC-WTC_000034949
Form detailing Method 508 parameters and sample volume information for environmental testing procedures.
Filed in the same folder
NYC-WTC_000034954
Reference data sheet listing concentrations of volatile organic compounds detected in sample AD28662.
Filed in the same folder
NYC-WTC_000034958
Calibration report showing recovery percentages for various chemical standards used in the GCMS analysis.
Filed in the same folder