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← Document results/DEP Box 22/GCMS X 11/24/01 A 12/4/01
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GCMS analysis comments for sample AD28662, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report noting contamination from the TurboVap concentrator and recovery rates for sample AD28662.

NYC-WTC_000034988–000034999

Folder label: “GCMS X 11/24/01 A 12/4/01”

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Scanned page image, NYC-WTC_000034995
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV2601\28680.D Vial: 11 Acq On : 28 Nov 2001 3:03 am Operator: 209 GALOS Sample : 11/24 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1,4-Dichlorobenzene-d4 Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 11.57 0.50 ug/1 108330 1,4-Dichlorobenzene-d4 11.69 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1, 4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 53 2 Benzene-1,2,3, 4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 25 3 Benzonitrile, 2 amino-5-chloro- 152 C7H5C1N2 005922-60-1 9 4 Benzofuran, 7-chloro- 152 C8H5C1O ____ 024410-55-7 9 Abundance 7 Scan 710 (11.566 min): 28680.D (-) Tm/z 149.90 100.00% 150

5000 115 78 - 52 38 87 1120 11.40 11.60 11.80 -H-H • ■ i ■ 3. 40 50 60 70 80 90 100 110 120 —l i.TTT 1 1— m/z 151.90 61.14% mz-> 30 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 150 *

5000 115 ............. ... ).................... 1120 11.40 11.60 11.80 52 78 m/z 114.90 34.99% 87 rnfz~> 30 35 ' • i •' • ■ i ■ ■ ' • i 40 50 111'1 ■ ■ 11 ■ 60 70 -PP ... ....... I 80 90 100 110 120 130 140 150 160 I—— Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 150 TP — 1 i 1 115 1120 11.40 11.60 11.80 5000 52 78 m/z 78.05 . 21.26%

35 87

miz-> 30 L 40 50 11 I 1 1 1 1 1 1 1 60 I i '' 1 11 ■' ' ■ i' ’ ' ’ i ■ ■ 70 80 90 100 110 120 130 140 150 160 1........ Abundance #10109: Benzonitrile, 2-amino-5-chloro- ............. -............. 152 11.20 11.40 11.60 11.80 m/z 52.00 15.58% 5000 125 63 90 117 I 98 ................ ........... .... ■ । ‘ 11 11 ■ ■ • i ■ i ■ ■ I ■ • ■ ■ i ■ • ■ ■ । m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80

28680.D GCMS1126.M Thu Dec 06 13:13:07 2001 Page 2

NYC-WTC_000034995

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NYC-WTC_000034995Source: NYC Law Department, mirrored locally

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