GCMS analysis results for sample AD28269, Nov 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\NOV2901\28263.D Vial: 33 Acq On : 29 Nov 2001 6:28 pm Operator: 209 GALOS Sample : 11/21 scan Inst : GC/MS 209 Mise Multiplrs 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1,4-Dichlorobenzene-d4 Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

11.56 0.51 ug/1 130387 1,4-Dichlorobenzene-d4 11.70

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 53 2 Benzene-1,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 17 3 2-Methyl-6-nitroaniline 152 C7H8N202I 000570-24-1 12 4 Benzofuran, 7-chloro- ______ 152 C8H5C10 024410-55-7 10 Abundance C Scan 710 (11.560 min): 28263.D (-) Tm/z 149.90 100.00% 1$0

5000 115 78 52 1120 11.40 11.60 11.80

m/z—> — 40 20 40 60 4464—44l80+—100— I... .... •......... 281 J 120 140 160 180 200 '226' 246 ' 260 280 m/z 151.90 59.71% Abundance #9593: 1,4-Dichlorobenzene-d4 150

5000 115 52 78 11.20 11.40 11.60 11.80 ' m/z 115.00 35.63% 35 . ..... - | I 1 ' ' ‘ i ' ■ •I11 ' I ■ ■ ' ■ l ■ ■ ■ ■ I''' ■ l ■ ■ ■ ■ I ■ ■ ■' I'''' I ■ ■ miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 150 TT" 115 1120 11.40 11.60 11.80 5000 52 78 m/z 78.05 . 19.92%

mz-> 20 35 .I ’ ■ i ■ ■ TITT 40 60 _........ i ' ■ ' 1 i 1 1 80 100 120 +- 140 160 180 200 220 240 260 280 Abundance #66883: 2-Methyl-6-nitroaniline 77 152 11.20 11.40 11.60 11.80...... m/z 52.00 14.50%

5000 106 52 94

m/z—> 20 2_1 40 60 ' ‘ i ’ ’ •' i 80 100 122135 M l 1 “ 1 • i * • 120 140 • i '' ' ‘ i11 ‘11 •1'11 160 180 200 220 240 260 280 ■ 1 - • > • । ■ i ■ ■ 11.20 11.40 11.60 11.80

28263.D GCMS1126.M Fri Nov 30 13:41:25 2001 Page 2

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