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GCMS analysis results for sample AD28269, Nov 2001

Machine-extracted title · confidence 95%

Laboratory report detailing GCMS analysis of sample AD28269 conducted on November 30, 2001.

NYC-WTC_000034180–000034197

Folder label: “GCMS X 11/21/01 A 11/27 - 11/28/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV2901\28263 .D Vial: 33 Acq On : 29 Nov 2001 6:28 pm Operator: 209 GALOS Sample : 11/21 scan Inst : GC/MS 209 Mise 2 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1-Monolinoleoylglycerol trimet Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 35.58 0.82 ug/1 121810 Perylene-dl2 37.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 40 2 Silanamine, N- XS6-dimethyl-4-[(tri 281 C14H27NOSi2 072088-09-6 22 3 3-Isopropoxv ,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 12 4 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 12 Abundance Scan 3326 (35.576 min): 28263. D (-) m/z 72.95 100.00% 73

147 5000 221 281 355 r r । . TTTrri . । TTTT 7 , r fTT . 429 35 20 35,40 35.60 35.80 36.00 39 117 , 177 1 11T 1 1 "IF r — ' — >7 1253,4327 L 401i —1901— T T । . . m/z 147.00 58.52% mz->_____ 50 100 150 200 250 300 350 400 450 500 550 Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether 73

207 5000 147 35.20 35.40 35.60 35.80 36.00

L.. 34 103 m/z 220.95 36.08% 281 ............................... ................. ,482............. , m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #39584: Silanamine, N-[2,6-dimethyl-4-[(trimethylsilyl)oxy] 73 281 209 35 20 35.40 35.60 35.80 36.00 5000 m/z 281.00 20.20% 45 251 . 179 120 147 | ----- • • । ■ miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim T T 1" 73 35 20 35.40 35.60 35.80 36.00 m/z 354.95 19.49% 5000 147

221 281 397 xi E ..... ................... 1.......1327........ 1........... 519 561 ' ' I ' ' ' ■ I ' 1 1 1 I ' ' 1 ' I ' ' ' ' I ' ' r' I ' ' ' 'I ' ■ ' ' I ' ' ' ' I ' ' ■ ' I ' ' ' ' I ' ■ m/z—> 50 100 150 200 250 300 350 400 450 500 550 35'20 35.40 35.60 35.80 36.00

28263.D GCMS1126.M Fri NOV 30 13:41:28 2001 Page 3

NYC-WTC_000034190

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NYC-WTC_000034190Source: NYC Law Department, mirrored locally

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