GCMS calibration table for TCLP analysis, Nov 2001

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Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.

NYC-WTC_000033911–000033935

Folder label: “GCMS X 11/20/01 A 11/26/01”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C: \HPCHEM\ 1 \DATA\ JAN0 802\28327.D Vial: 5 Acq On 8 Jan 2002 4:16 pm Operator: 209 GALOS Sample 508 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C: \DATABASE\NBS75K. L ********************************************************************* Peak Number 15 1-Monolinoleoylglycerol trimet Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T.

35.43 1.92 ug/1 453817 Perylene-d12 36.91

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 1-Monol inoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 45 2 Trisiloxane, 1, 1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 32 3 Silanamine, N-J 2,6-dimethyl-4-[(tri 281 C14H27NOSi2 072088-09-6 25 4 Butanoic acid/ 3-methyl-2-oxo-, bis 260 C11H2403Si2 072361-19-4 23 Abundance Scan 3309 (35.425 min): 28327.D (-) m/ Z 73.00 100.00% 73

147 5000 221 281 355 i ■ ■ ■ ■ i ■ • I ‘ 1 1 ' I ‘ ' ' I I I I I 253... , 327 401 429 35.00 35.20 35.40 35.60 35.80 45 T" i" 96 117. 'i ■ ■ — 4 i > 1914— r TTT । । “i —T i r । f । । r . । , m/z 147.00 52.55% m/z-> 50 100 150 200 250 300 350 400 450 Abundance #58871; 1-Monolinoleoylglycerol trimethylsilyl ether 73 — — , 207 5000 147 35.00 35.20 35.40 35.60 35.80 34 103 m/z 221.05 30.78% 281 395 482 miz-> 50 100 150 200 250 1 300'1350 ‘ ' 400 * 450 Abundance #74103 Trisiloxane, 1.1,1,5.5,5-hexamethyl-3,3-bis[(trimet 73 .............. — 147 1 1 1 1 ' 35.00 35.20 35.40 35.60 35.80 5000 m/z 281.00 17.71% 281 45 369 I j. 117 i 207 249. | Tf . I..' . Tn—ma I I | ! . TTTTTTTT T .. '..T.. 1.. ’ m/z-> 50 100 150 200 250 300 350 400 450 Abundance #39584: Silanamine, N-[2,6-dimethyl-4-[(trimethylsilyl)oxy] I ’ ■ I ■ ' ■ ' I ■ . ' ' I ' ■ ' I 1 • 73 35.00 35.20 35.40 35.60 35.80 281 m/z 355.05 15.50% 209 5000 45 251 .. 179 125 14 7 I —. T. ,. r. ,. .. --. ,. ,. —. .. ,. ,.— f ' t 1 1 ‘ ' i • • T-r-p-r-r-r-r-r-r-r miz-> 50 100 150 200 250 300 350 400 450 35.00 35.20 35.40 35.60 35.80

28327.D GCMS1126.M Wed Jan 09 09:15:49 2002 Page 15

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