GCMS comments for sample AD28666, Dec 2001

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV2901\28666.D Vial: 35 Acq On : 29 Nov 2001 8:26 pm Operator: 209 GALOS Sample : 11/23 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Paramss LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L \ ********************************************************************* Peak Number 1 1,4-Dichlorobenzene-d4 Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 11.56 0.49 ug/1 101753 1,4-Dichlorobenzene-d4 11.70

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1, 4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 53 2 Benzenamine, N-methyl-4-nitro- 152 C7H8N202 000100-15-2 14 3 Benzene-!/; 2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 12 4 2-Methy^-6-nitroaniline 152 C7H8N202: ____ 000570-24-1 10 Abundance Scan 710 (11.561 min): 28666.D (-) m/z 149.90 100.00% 150

5000 115 52 78 11 20 11.40 11.60 11.80 11 । 38 I J , I i'I'i -H 11111 4 .. .. । . 1 207 281 m/z 151.90 . 65.25% m/z--> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #9593:1,4-Dichlorobenzene-d4 150

5000 115 78 11.20 11.40 11.60 11.80....... 52 m/z 115.00 38.95% — 35 J Il miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 I ’ ' ' ' I ’ ' r' I ' ' ' ’ I 1 ’ ' ' I ■ ' ' ' I • ‘ ' I TTT I | I > I I | ! I

Abundance #10120: Benzenamine, N-methyl-4-nitro- 1$2

77 122 11.20 11.40 11.60 11.80 ' 110 5000 m/z 77.95 . 19.78% 65

miz-> 20 30 I—4 40 60 LM 80 94 ,

100 120 140 160 180 200 220 240 260 280 Abundance #9592: Benzene-1,2,3,4-44-, 5,6-dichloro- TTIr 150 11.20 11/40 11.60 11.80 m/z52.0016.04% 115 5000 52 78

.... — 4........... 35

miz-> 20 | 40 ' I 1' 60 80 Lt.... 100 120 140 160 180 200 "22Q 240 260 280 11 Iso' 1140 11.60 11.80.....

28666.D GCMS1126.M Fri Nov 30 16:21:58 2001 Page 1

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