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GCMS analysis results for sample AD24480, Nov 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD24480 conducted on November 14, 2001, identifying unknown compounds.

NYC-WTC_000068529–000068543

Folder label: “GCMS Scan X 10/12/01 An 11/3/01

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Scanned page image, NYC-WTC_000068542
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\NOV0 201\24480.D Vial: 18 Acq On 3 Nov 2001 7:34 am Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 1,4-Dichlorobenzene-d4 Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 11.57 0.51 ug/1 70363 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 72 2 Benzene-1,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 30 3 Benzenamin^, 2-methyl-4-nitro- 152 C7H8N2O2 000099-52-5 14 4 Benzenamine, 2-methyl-5-nitro- 152 C7H8N2O2 000099-55-8 10 Abundance I Scan 711 (11.572 min): 24480. D (-) m/z 149.90 100.00% 1$0

aaS 115 78 52 40 11.20 11.40 11.60 11.80 12.00 ' ' I ' ' ‘ ' I ''' m/z 151.90 65.63% v/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 150

115 T-|—r-r-r-r-p—r ' ' I' '

78 11.20 11.40 11.60 11.80 12.00 52 m/z 114.90 38.35% 35 TT^-> 30 40 50 ' 60 70 80 ' ' I ‘ 90 ' I ' ‘ ' I ' ' J............ 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5.6-dichloro- 1$0 ' I ' ' ' ' 1 ' 115 11.20 11.40 11.60 11.80 12.00 5000 52 78 m/z78.05 23.89%

•nfe-> 30 35 I 40 50 60 70 80 X,.,. ..... I,i„, 90 100 110 120 130 140 150 160 Abundance #10129: Benzenamine. 2-methyl-4-nitro- 77 106 152 11 20 11.40 11.60 11.80 12.00 m/z 52.00 15.01%

5000 51 94

Il ? Ill . , 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00

24480.D NP103001.M Tue Nov 13 10:12:57 2001 Page 6

NYC-WTC_000068542

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NYC-WTC_000068542Source: NYC Law Department, mirrored locally

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