Laboratory report noting contamination from the TurboVap concentrator and recovery rates for sample AD28662.
NYC-WTC_000034988–000034999Folder label: “GCMS X 11/24/01 A 12/4/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV2601\28680.D Vial: 11 Acq On : 28 Nov 2001 3:03 am Operator: 209 GALOS Sample : 11/24 scan Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 38.02 1.26 ug/1 114404 Perylene-d12 37.12
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Trisiloxane, 1,1.1, 5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 46 2 Ethanedioic acid, bis(trimethylsily 234 C8H18O4S12 018294-04-7 25 3 Cyclopropanamine, N-methyl-l-phenyl 147 C10H13N 056771-48-3 22 4 3,6-Dioxa-2, ,5,7-tetrasilaoctane, 294 C10H3002Si4 004342-25-0 17 Abundance 7 Scan 3592 (38.024 min): 28680.D (-) m/z 73.00 100.00% 73 147
221 5000 281 355 429 37.60 37.80 38.00 38,20 38.40 36 Tt So - 96.117 ।. r..3271 A1.234. th_.. TT’TTT —9. TTTTTI‘‘..1‘401 7 1 TTETTT m/z 146.95 84.79% m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147
5000 281 37,60 37.80 38.00 38.20 38.40 m/z 220.95 53.02% 45 369 _/ _ 207 249 . , ........ 117...... TIUUCTTTTTTT ।1p k1(।...j r1111■11111 “uII—T——1"00VUTTTar miz—> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #30580: Ethanedioic acid, bis(trimethylsily!) ester 73 147 I TTETLT I 'I I I I irlJ I 1 1 TT 1 3760 37.80 38.00 38.20 38.40 5000 m/z 281.00 26.78% 45
mmmmml 190 219 ■■|IIII|I H | . I ■ I | I I .. | .. M | | | | | I|IIII|!HI|I m/z—> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #9103: Cyclopropanamine, N-methyl-1-phenyl- 147 37.60 37.80 38.00 38.20 38.40 m/z 355.05 24.29% 5000
42 6492120 . .......................... \ A m/z—> 40 60 80 100120 140 160 180 200 220 240 260 280300 320 340 360 380 400 420 T 37.60 37.80 38.00 38.20 38.40
28680.D GCMS1126.M Thu Dec 06 13:13:09 2001 Page 3
NYC-WTC_000034996
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NYC-WTC_000034886
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28479 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034808
Laboratory analyst notes on GCMS scan results, recovery rates, and low pH conditions for sample AD28649.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034819
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034198
Laboratory report detailing GCMS analysis of sample AD28263 conducted between November 21 and 26, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034180
Laboratory report detailing GCMS analysis of sample AD28269 conducted on November 30, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034213
Laboratory report detailing GCMS analysis of sample AD28271 conducted on December 6, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034830
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034331
Laboratory report documenting GCMS analysis of sample AD28427 conducted between November 21 and 26, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033765
Analytical commentary for sample AD28149 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033834
Analytical commentary for sample AD28155 dated November 29, 2001, noting detection of bis(2-Ethylhexyl)phthalate and low recovery rates.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000004149
Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033800
Analytical commentary for sample AD28157 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000034946
Laboratory report detailing GCMS scan results for sample AD28650, noting phthalate detection and low pH.
Filed in the same folder
NYC-WTC_000034947
Document containing unreadable text or corrupted data from the Department of Environmental Protection archives.
Filed in the same folder
NYC-WTC_000034949
Form detailing Method 508 parameters and sample volume information for environmental testing procedures.
Filed in the same folder
NYC-WTC_000034954
Reference data sheet listing concentrations of volatile organic compounds detected in sample AD28662.
Filed in the same folder
NYC-WTC_000034958
Calibration report showing recovery percentages for various chemical standards used in the GCMS analysis.
Filed in the same folder