GCMS analysis results for sample AE04129, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAR2202\4129.D Vial: 25 Acq On : 23 Mar 2002 7:44 pm Operator: Sample : gc/ms scan 2/25 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Methyl-4-bromo-l-butene Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

6.59 1.94 ug/1 223654 1,4-Dichlorobenzene-d4 12.26

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Methyl-4-bromo-1-butene 148 C5H9Br 020038-12-4 78 2 2-Butene, 1-bromo-3-methyl- 148 C5H9Br 000870-63-3 74 3 Cyclopentane, bromo- 148 C5H9Br 000137-43-9 45 4 1-Butene, 3,3-dimethyl- 84 C6H12 000558-37-2 43 Abundance Scan 168 (6.591 min): 4129.D (-) m/z 69.00 100.00% 41 69

5000

53 6.20 6.40 6.60 6.80 7.00 '111'111 ■ l ' 1, ■ 62.1 81 109 133 148 T—uuuuTmuummOTmTmROr m/z 41.00 85.22% miz-> 20 30__ 40_ 50__ 60_ 70 80 90 100 110 120 130 140 150 Abundance #9146: 2-Methyl-4-bromo-1 -butene 69

41 5000 14/4/11 4$1* ■ 1 ■ 5tt । 11 6.20 6.40 6.60 6.80 7.00 55 27 148 m/z 24.44% T-p-r-n-p-r-n-f Hr • i • • ■ ‘ i ■ 1 miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance d65o8. 2-Sutene, *-bromo-d-cttyi- 41 69 TI17r PPP 6.20 6.40 6.60 6.80 7.00 5000 m/z 53.00 12.67% 27 53 148 ■ i ■ • ■ ■ i ■ ■ ■ ■ i1 ■ ■ ■ i ■1 ■ ■ i ‘ I1dnum]uuut!—0pnoBup——nor '11' m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #9144: Cyclopentane, bromo- ■ I • > ■ • l " • > 1 1 0 •■ ' ‘ i ■ ■ 69 6.20 6.40 6.60 6.80I 7.00 m/z 66.95 7.20% 41 5000

m/z-> +20 27

30 40 53 11 ■ ■ 50 60 81 70 80 90 100 110 120 130 140 150 121 148 6.20 6.40 ............. 6.60 6.80 7.00

4129.D GCMS0308.M Wed Mar 27 10:06:13 2002 Page 1

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