GCMS unknown compound analysis, sample AE05515, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\APR0102\5515.D Vial: 6 Acq On 1 Apr 2002 4:11 pm Operator: Sample gc/ms scan 3/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Methyl-4-bromo-1-butene Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

6.58 5.09 ug/1 859216 1,4-Dichlorobenzene-d4 12.25

Hit# of 5y Tentative ID MW MolForm CAS# Qual

1 2-Methyl-4-bromo-1-butene 148 C5H9Br 020038-12-4 64X 2 2-Butene, l-bromo-3-methyl- 148 C5H9Br 000870-63-3 50 3 Meparfynol 98 C6H10O 000077-75-8 45 2~Bnt^ne, 3,3-dimethyl-_________ 84 C6H12 _________ 00255822222 4 3 lAbmdance 7 / " 41 Scan 167(6.576min): 5515.D{-) 69 m/z 69.10 ‘100.00%

5000

...................... A , I, 53 6.20 6.40 6.60 6.80 7.00 O-l .. ............ 62, I I 79 93 107 119 135 148 p-TT-7YTT-rTyTT-rTjT-r-rT-p-TT-q-T-T-TT-p-^^ m/z 41.0,0 86.52% m/z-> 10 20 30 40 50 60 70 801 90 100 110 120 130 140 150 'Abundance #9146: 2-Methyl-4-bromo-1-butene 6l9

41 ............ 5000 6.20 6.40 6.60 6.80 7.00 55 27 148 m/ z 39.05 23.50% ...... !.... I .......... I.............................. Ijn hi/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #66538: 2-Qutene. 1-broino-3-rriefliyl- 4!l 69

6.20 6.40 6.60 6.80 7.00 5000 m/ z 53.00 12.81% 27 53 I 148 I'''' I' m/2->10...20 .. 30 40__ 50__ 60 _70__80 90 100 110 120 130 J40__ 150 Abundance #63208: Meparfynol .......... , e|9 6.20 6.40 6.60 6.80 7.00 m/z 67.05 6.20% 5000 43

83 27 53

hi/z~> .AnX 97 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 6.20 6^ 6,60 6.80 7.00

5515.D GCMS0403.M Thu Apr 04 13:52:50 2002 Page 1

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