GCMS analysis results for sample AE04131, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAR22O2\4131.D Vial: 27 Acq On : 23 Mar 2002 9:42 pm Operator: Sample : gc/ms scan 2/25 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 3-Hydroxy-3-methyl-2-butanone Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

7.30 1.27 ug/1 145804 1,4-Dichlorobenzene-d4 12.26

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hydroxy-3-methyl-2-butanone 102 C5H10O2! 2 2-Hexanone, 3 -hydroxy- 3,5-dimethyl- 144 C8H16O2! 3 Propane, 2-ethoxy-2-methyl- 102 C6H14O 000115-22-0 42 006321-14-8 38 000637-92-3 36 4 2-Propanol, 2-methyl-_____ _____________ 74 C4H10O _ ___ 000075-65-0 36 Abundance ”

5000 7.... Scan 245 (7.296 min): 4131 .D (-)

43 59 " "T 107 7.00 7.20 7.40 7.60 i . . ।... . ). ,. ., . +3844 53 1**174’17 65 71 87 111 > > > > i m/z 43.05 43.05% m/z->___ 10___ 20 30 40 50 60 70 80 90 100 110 Abundance #63477: 3-Hydroxy-3-methyl-2-butanone 59

5000 31 *3 r i ■ 1 rPrpi -2 43 7.00 7.20 7.40 7.60 15 m/z 107.00 17.77% 87 Pmm* **I 69 ' i ■ ' • ■ i ■ ‘ ' ■ i ‘ 102 ‘ * i • ' ‘ ' I • ‘ ■ ■ i . miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance "$£36: 2-HPerone 3iurxy3 5-dimethet 59 ————033 7.00 7.20 7.40 7.60 5000 m/z 41.05 17.48.% 43 . 101 69 83 111 ‘ ■ i 1 • • ‘ i ■ ■ ■ 1 I ■ ■ ' ■ I ' ' ‘ ' I ■ ■ ■ 1 i ■ ■ ‘ 1 i ■ • ' 1 i • ■ ' ‘ i ' 1 ■ ■ i 1 • 1 ■ i • ‘ ■ ■ i m/z-> 10 20 30 40 50 60 70 80 90 100 110__ _ Abundance #63580: Propane, 2-ethoxy-2-methyl- 112TTRT 59 7.00 7.20 7.40 7.60 m/z 71.00 7.03% 5000 .87 41 31 | *‘I***I*‘)**I 1 I1 • ■ ‘ l ‘ T TmmB—BmBTTr . W m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.00 7.20 7.40 7.60

4131.D GCMS0308.M Wed Mar 27 10:09:51 2002 Page 2

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