GCMS analysis results for sample AE10891, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C : \HPCHEM\ 1 \DATA\MAY1 502\10891.D Vial: 9 Acq On : 15 May 2002 9:54 pm Operator: Sample : GC/MS SCAN 5/10 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 1 3-Buten-2-ol, 2-methyl- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 7.01 2.02 ug/1 125405 1,4-Dichlorobenzene-d4 12.16 Hit# of Tentative ID MW MolForm CAS# Qual

1 3-Bucen-2-ol, 2-methyl- 86 C5H10O 000115-18-4 45 2 B enol, methyl- 86 C5H10O 060766-00-9 42 3 pentane, 2-bromo- 150 C5HllBr 000107-81-3 38 4/Oxi rane, propyl -_________________ 86 C5H10O 001003-14-1 32 undance Scan 215 (7.014 min): 10891 .D (-) m/z 43.05 100.00% 43

71 5000 55 j

6.60 6.80 7.00 7.20 7.40

m/z-> — 3 87 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 ■ i ■ 1’’ ) > > ‘ 11 > < < 11111) ।> 11!) 111 > ।,) 111 m/z 41.05 97.73% Abundance #62855:3-Buten-2-ol, 2-methyl- 43 71

5000 59 6.60 6.80 7.00 7.20 7.40 27 m/z 71.10 59.91%

m/z-> 10 ....... I. .1... + — 86 20 30 40 50 60 70 80 90 100 110 120 130 140 150 , I PuHpOuotpuum9*)"9]nunn

Abundance #698: Butenol, methyl- 43 71 6.60 6.80 7.00 7.20 7.40 5000 59 m/z 69.05 57.39% 27 15 ..................... .

miz—> 10 20 30 40 51460 II70 80 8690 100 110 120 130 140 150 50 , I

Abundance #66675: Pentane, 2-bromo- 43 6.60 6.80 7.00 7.20 7.40 71 m/z 55.00 32.49% 5000 27 55

T-rj-r --H-H 1'11' ■ " i'' " I 1'' ■ i ■' ■' i ■1 • ■ i ■''107■ i ■' ■11123 ■'' 150 i'1 ■' i'111 r 1 . A..... m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 6.60 6.80 7.00 7.20 7.40

10891.D GCMS0510.M Fri May 17 10:17:30 2002 Page 1

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