GCMS analysis results for sample AE10892, May 2002

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Data File : C:\HPCHEM\l\DATA\MAY1502\10892.D Vial: 10 Acq On : 15 May 2002 10:52 pm Operator: Sample : GC/MS SCAN 5/10 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 Butenol, methyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

7.01 0.96 ug/1 56362 1,4-Dichlorobenzene-d4 12.16 Hit# of Tentative ID MW MolForm CAS# Qual

1 Butenol , methyl - 86 C5H10O 060766-00-9 47 2 1,6-Heptadien-4-ol 112 C7H120 002883-45-6 42 3/1-Heptene, 4-methyl- 112 C8H16 013151-05-8 38 /4 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 38 Abundance Scan 215 (7.015 min): 10892. D (-) m/ z 43.05 100.00% 43 71 5000 55 6.60 6.80 7.00 7.20 7.40 ----- 36 ++494 44 l 84 • i ■ i ‘ • i ■ ■ ■ ■ i ■ ■ ■ - i ■ m/z 41.10 92.05% m/z-> 10 20 30 40 50 60 70l 80 90 100 110 Abundance #698: Butenol, methyl- 43 71

5000 59 27 6.60 6.80 7.00 7.20 7.40 15 m/z 71.10 66.71% 53

miz—> 10 20 30 p 50l, 60p 40 — 70 80 86........... 90 100 110 Abundance #2591:1,6-Heptadien-4-ol 4)3

71 6.60 6.80 7.00 7.20 7.40 5000 m/z 69.05 53.76% 27 53 79 *0——— । " l"......'I1' 1 ■ ■ > i ■ • • ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i > ■ < ■ । mz-> 10 20 30 40 50 60 70I 80 90 100 110 Abundance #2675:1-Heptene, 4-methyl- 43 6.60 6.80 7.00 7.20 7.40 70 m/ Z 55.00 31.67%

5000 55

27

m/z—> ■ ' । ■ 1 1 1 । 1 ■ * 1 । ■ ■ ■ < । 10 20 30 40 -4pl 50 60 70 TT 90 112 100 110 80 84 1 । ■ ■ ■ ■ । 'r ' । ■ 1 ■ ■ । ..... ................. 6.60 6.80 7.00 7.20 7.40

10892.D GCMS0510.M Fri May 17 10:24:41 2002 Page 1

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