GCMS analysis results for sample AE10892, May 2002

NYC 9/11 Public Portal Document Library searcn compound Report

Data File : C:\HPCHEM\l\DATA\MAY1502\10892.D Vial: 10 Acq On : 15 May 2002 10:52 pm Operator: Sample : GC/MS SCAN 5/10 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Oxirane, (3-methylbutyl)- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 7.79 0.64 ug/1 37505 1,4-Dichlorobenzene-d4 12.16 Hit# of/ 5 Tentative ID MW Mol Fo rm CAS# Qual

1 Oxirane, (3-methylbutyl)- 114 C7H140 053229-41-7 25 2 Pentane, 2-bromo- 150 C5HllBr 000107-81-3 25 3 1-Butanol, 2,3-dimethyl- 102 C6H140 019550-30-2 23 /4 l-Hydroxy-3-methyl-2-butanone 102 C5H10O2 036960-22-2 17 Abundance Scan 300 (7,794 min): 10892.D (-) m/z 41.15 100.00% 41

5000 71 ' i 1 ■ > ।— r . r । । i .< . । . 38 45 49 53 58 7.40 7.60 7.80 8.00 8.20 67 1 84 m/z-> 1 20 25 30 35 - - 11 ■1' ■ i ■ 40 45 50 55 60 65 70 75 80 85 90 ■'111' '' i''' ■ i m/ z 43.05 68.06% Abundance #3027: Oxirane, (3-methylbuty!)- 4|1

56 71 5000 7.40 7.60 7.80 8.00 8.20 m/z 39.10 43 .20% 44

m/z-> ■ ‘ ■ i ■ ■1 ■ i ■' ■ ■ i " 1 ■ i1 ■ ■ ■ i

20 25 30 35 40 H —9 45 50 55 60 65 70 75 81 85 ■' i11 1' i'' ■ ■ i11 ■ ■ i 80 85 90 Abundance #9581: Pentane, 2-bromo- 43 27 7.40 7.60 7.80 8.00 8.20 5000 39 m/ z 71.10 41.25% 71

53 57 mz-> ■'111mll.3°... Il 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 11'1'11 ■'1~ i ■' “ i'1'' i' ----PPP

Abundance #1776:1-Butanol, 2,3-dimethyl- / 43 7.40 7.60 7.80 8.00 8.20 m/z 69.05 39.65% 71 5000 27 31 84

■' i1' ■ ■ i ■ - 5659 ■ i ■''11'' i'''' i' " ' i -- miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 7.40 7.60 7.80 8.00 8.20

10892.D GCMS0510.M Fri May 17 10:24:41 2002 Page 2

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