GCMS analysis results for sample AE10851, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C: \HPCHEM\1\DATA\MAY1502\10851.D Vial: 6 Acq On : 15 May 2002 6:58 pm Operator: Sample : GC/MS SCAN 5/10 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 1 3-Buten-2-ol, 2-methyl- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 7.02 0.88 ug/1 50558 1,4-Dichlorobenzene-d4 12.16 Hit# O 5 Tentative ID MW MolForm CAS# Qual

1 Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 52 'Oxirane, (3-methylbutyl)- 114 C7H140 053229-41-7 47 Butenol, methyl- 86 C5H10O 060766-00-9 40 4 l-Heptene, 4-methyl- 112 C8H16 013151-05-8 33 Abundance Scan 216 (7.019 min): 10851 .D (-) m/z 43.05 100.00% 43 71 5000 55

37 129 6.60 6.80 7.00 7.20 ' 7.40 86 1 ' । 1 ' ' 1 I 1 1 1 1 I 1 ' (I1 I TH i ■ 1 ■ 1 i 1 1 1 ' i ■ ■ ■ ' 1 1 1 1 1 । 1 1 ' m/z 41.05 94.45% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #62855:3-Buten-2-ol, 2-methyl- 43 7

5000 PPA 1 11TTIIIII 59 6.60 6.80 7.00 7.20 7.40 27 ... I.... + m/z 71.10 62.65% 53 86 ■ ■ । ■ 1 1 i ■ ■ ' ■ 1 1 1 ' 1 1 1 —111' i ■ ■11111 ' n 1 1111r 11111 1'111' mz-> 10 20 30 40 50 60 70> 80 90 100 110 120 130 Abundance #3027: Oxirane, (3-methylbutyl)- 41 N

6.60 6.80 7.00 7.20 7.40 5000 56 71 m/ z 69.05 57.10%

81 ' ' i ' ' ■ ■ i ■ ■ ■ 1 1 ■ 1 ' 1 i1 "’Trr"’11111111111111*TT1171111111TII0"T mlz-> 10 20 30 40 60 70 80 90 100 110 120 130 ... ................. Abundance #698: Butenol, methyl- 43 71 6.60 6.80 7.00 7.20 7.40 m/z 55.00 31.85% 5000 59

. AW_ 27 15 53

Tl/Z-> ' ' I ' 1 10 ... . ... ... .1,1, ।,,, 1 ■ ।' ■ ■ ■ । ■ ■' ■ i''1 ■ । ■ ■ ■11 ■'

20 30 40 50 60 +70)1 80 90 100 110 120 130 6.60 6.80 7.00 7.20 7.40

10851.D GCMS0510.M Fri May 17 09:52:53 2002 Page 1

NYC-WTC_000024216