GCMS analysis results for sample AE11602, June 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C: \HPCHEM\ 1 \DATA\MAY2102\11602.D Vial: 31 Acq On : 22 May 2002 8:06 pm Operator: Sample : EXTRACTS/20 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0520 .M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 15 2-Propenoic acid, 2-methyl-, o Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 13.40 2.36 ug/1 151356 1,4-Dichlorobenzene-d4 12.15

Hit# Of 5 'entative ID MW MolForm CAS# Qual

1 2-Propenoic acid, 2-methyl-, octyl 198 C12H2202I 002157-01-9 17 2 1-Butanol/ 3-methyl-, acetate 130 C7H14O2 000123-92-2 12 3 4-Methyl/2-hexene,c&t 98 C7H14 003404-55-5 9 4 Ethyl Acetate Abundance 88 C4H8O2 000141-78-6 9 Scan 912 (13.401 min): 11602.D (-) m/z 69.05 100.00% 43 69

5000

55 61 98 Lt JM • ■ i ■ ■ 13.00 13.20 13.40 13.60 13.80

miz-> 20 ............ 1, 30 40 .49.1070 Phi, 50 60 70 80 87 90 100 111 119 129 110 120 130 m/z 43.05 91.40% Abundance #22430:2-Propenoic acid, 2-methyl-, octyl ester 69

5000 57 ANVW/... 13.00 13.20 13.40 13.60 13.80 83 m/z 70.05 41.70% 42 112

miz-> 20 30 1 40 ....50 . •60i • • 70 +1 80 90 99 • • । * * ■ ■ । 100 110 ■ j i ■ ■. ।... ■ । 120 130 .

Abundance #65212:1-Butanol, 3-methyl-, acetate 43 T 1 ‘ l ■ ■ 13.00 13.20 13.40 13.60 13.80 5000 70 m/z 41.05 41.21% 55

17 61 —L 87

AM , I 130 • ’ i • Il p ■ i ■ ■ ■ ■ i ‘ ■ i ■ ■ ■ ‘ i 1 1 ■ ■ i • ■ miz—> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #1318:4-Methyl-2-hexene,c&t 1 1 1 1 1 41 69 13.00 13.20 13.40 13.60 13.80 m/z 98.10 18.83%

5000 55

miz—> 27

• 1 1 1 " I ' ' 1 ' I 20 30 40 +50 ....... il 60 70 , 80jopos 90 83

100 110 120 130 98

1 i ■ • ■ ‘ i ■ 1 ■ ■ i • ■ ■ • i ■ ■ AAM/ ' ■ i ' ‘ 13.00 13.20 13.40 13.60 13.80

11602.D GCMS0520.M Fri May 24 08:33:18 2002 Page 15 NYC-WTC_000013962